MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Application of Modified Optical Indentation Microscopy as New In Situ Indentation Method
Takahiro MinetaSeiji MiuraKazuhiko OkaTatsuya Miyajima
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JOURNAL FREE ACCESS Advance online publication

Article ID: MD201904

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Abstract

In the present study, a newly established in situ indentation technique by the use of an optically transparent indenter and an immersion liquid, so-called “modified optical indentation microscopy”, was applied for an investigation on the plastic deformation behavior of various samples during indentation. In this technique, the gap between the indenter and the specimen surface is filled with the immersion liquid such as silicone oil and kerosene to widely observe the specimen surface during indentation. In the in situ observations by this technique using polycrystalline pure Mg, the occurrence of various plastic deformation mechanisms and the increase of the anisotropic contact area during indentation can be recognized. Moreover, the increase and the decrease of the contact area which is corresponding to superelasticity during indentation were observed by this technique using the TiNi superelastic alloy. The results of the in situ observations were consistent with the analysis results based on the Hertz theory.

Fig. 3 (a–f) In situ images, (g) an optical micrograph after testing, and (h) EBSD analysis results of polycrystalline pure Mg. The red circles in (b) indicate the twins. Fullsize Image
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© 2019 The Japan Institute of Metals and Materials
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