Preprints of Annual Meeting of The Ceramic Society of Japan
Preprints of Fall Meeting of The Ceramic Society of Japan
Preprints of Annual Meeting of The Ceramic Society of Japan, 2003
Session ID : 2I13
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Synthesis of β-SiAlON by carbothermal reduction-nitridation of zeolite
*Fengjin LiJunichi TatamiTakeshi MeguroKatsutoshi Komeya
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Abstract
Zeolite and carbon powders were mixed in ethanol for 1hour. After the slurry was dried, the powder mixture was fired at the temperature of 1450°C for 2hours in 0.5l/minN2 flow, followed by heat-treatment at the temperature of 700°C for 2hours in air in order to remove residual carbon. As a result, it was confirmed that the main phase of synthesized powder was β-SiAlON from XRD analysis and it was composed of ultra fine particles from SEM observation and measurement of specific surface area. Consequently, zeolote is very useful raw material to synthesige very fine β-SiAl0N powders.
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© The Ceramic Society of Japan 2003
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