Phosphorus Research Bulletin
Online ISSN : 1882-2363
Print ISSN : 0918-4783
ISSN-L : 0918-4783
EFFECT OF HYDROTHERMAL TREATMENT ON PREPARATION OF TRANSPARENT APATITE CERAMICS BY SPARK PLASMA SINTERING
Daisuke KawagoeYoshihiro KogaNakamichi YamasakiHirotaka FujimoriSeishi GotoKoji Ioku
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2004 年 17 巻 p. 240-245

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Calcium hydroxyapatite, Ca10(PO4)6(OH)2: HA, is the inorganic principle component of natural bones and teeth, The present study deals with the preparation of HA ceramics with a different OH amount by spark plasma sintering (SPS) from HA fine crystals synthesized hydrothermally. The dense hydroxyapatite ceramics with controlled OH were prepared at the temperatures from 800°C to 1000 °C for 10 min. Transparent hydroxyapatite ceramics were prepared by SPS at 900 °C and 1000 °C. The amount of OH ion in the structure of hydroxyapatite was decreased with increasing temperature of sintering. The hydrothermally treated HA fine crystals have the high sinterability.

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© Japanese Association of Inorganic Phosphorus Chemistry
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