X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 9
Crystal Structure of Isothiocyanato-N,N′-dimethyl-N,N′-bis(pyridine-2-ylmethyl)propane-1,3-diaminecopper(II) Perchlorate
Takashi YOKOYAMAMasakazu YOSHISEShintaroh HASEAyumi KAWATEHaruo AKASHIMichio ZENKI
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電子付録

2011 年 27 巻 p. 51-52

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抄録
The complex of an isothiocyanato-N,N′-dimethyl-N,N′-bis(pyridine-2-ylmethyl)propane-1,3-diaminecopper(II) perchlorate ([Cu(NCS)(LMe2)]ClO4) was prepared. Its crystal structure was determined by X-ray diffractometry. [Cu(NCS)(LMe2)]ClO4 crystallized in a triclinic system, and was characterized thus: P1, a = 9.257(3), b = 9.883(4), c = 11.806(5)Å, α = 89.638(12), β = 81.053(10), γ = 88.841(12)°, Z = 2, V = 1066.7(7)Å3. The crystal structure was solved by direct methods and refined by full-matrix least squares on F2 to final values of R1 = 0.058.
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© 2011 by The Japan Society for Analytical Chemistry
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