X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 1
Rhenium Complex with 2-[(2-Pyridylmethyl)amino]ethanethiol
Masahiro MIKURIYATetsuji WATANABEAiko SUYAMADaisuke YOSHIOKA
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2015 年 31 巻 p. 3-4

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抄録
A rhenium(VII) complex with 2-[(2-pyridylmethyl)amino]ethanethiol (Hpmaet), [Re(pmaet)O3], was synthesized. The crystal structure was determined by the single-crystal X-ray diffraction method at 123 K. It crystallizes in the monoclinic space group P21/n with a = 10.054(5)Å, b = 8.466(4)Å, c = 12.924(7)Å, β = 108.552(9)°, V = 1043.0(10)Å3, Dx = 2.557 g/cm3, and Z = 4. The R1 [I > 2σ(I)] and wR2 (all data) values are 0.0195 and 0.0545, respectively, for all 2401 independent reflections. The compound consists of an octahedral molecule of rhenium(VII) with facial pmaet and three oxido oxygens.
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© 2015 by The Japan Society for Analytical Chemistry
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