抄録
The structure of 4-hydroxy-3-methoxybenzaldehyde-4-methylthiosemicarbazone (VAMTSC) was determined by X-ray crystallography. The molecular structure matches the asymmetric unit, and the compound crystallizes in a monoclinic system. It was characterized thus: P21/c, a = 8.4960(3), b = 8.5040(2), c = 17.2236(6)Å, β = 111.513(2)°, Z = 4, V = 1157.71(6)Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0403 and wR2 = 0.078.
