Experimental work on liquid-liquid spray columns is presented, which includes 56 runs in 2.92cm. and 5.64cm. I.D. glass towers, where the mass transfer does not occur. The behavior of the dispersed phase projected from the various nozzle tips is observed over a wide range of velocity at the tip (5-200cm/sec), and the hold-up is measured under the following conditions up to the flooding.
Systems: Four kinds of mineral oils and water
Dispersed phase: Both oils and water, alternatively 
Tip dimensions: 0.50, 0.90, 1.50, 3.05 and 5.00mm. I.D., 1, 2, 3, 7, and 13 points. (No-tip plate type distributor is also used.)
Flow rates (Superficial velocity based on the tower cross-section):
Dispersed phase (U
D): 2-60m
3/m
2hr 
Continuous phase (U
C): 0-110m
3/m
2hr U
C/U
D: 0.3-36 
Viscosity of both phases (μ
C and μ
D): 0.8-300c.p. 
Density difference (Δρ): 0.075-0.117gr/cub.cm.
Interfacial tension (σ): 34.0-52.7dyne/cm 
Temperature: Room temperature (7-31°C)
The results obtained here are summarized as follows: 1) Distributor nozzles and projecting velocities.
The observed drop formation is classified into three stages according to the projecting velocities of the dispersed phase. The first stage is in the range of We=au
D2ρ
D/σ<2, where the drop forms one by one at the tip. The second stage, where the uniform drops form from a stream projected, is in the range of u
D<100cm/sec. In the third stage, u
D>100cm/sec, the size of drops become non-uniform probably due to the turbulence in the nozzle tube. It is also observed that no-tip plate type distributor is not satisfactory, because the dispersed phase tends to wet the surface of the plate, and forms large irregular drops. The large tip diameter (a=0.50cm) is also unsatisfactory, since the flooding occurs at low velocity.
2) Hold-up 
The percentage hold-up, ε, is generally correlated with some demensionless groups as shown in Fig. 4-Fig. 6. The ordinate of Fig. 6 is (1+U
C/U
D)
0.4(1-a/D)
2ε, and the abscissa is (1+UC/U
D)
0.5(U
D/√ga) for √β>25, and is (2.3/β
0.13)(1+U
C/U
D)
0.5(U
D/√ga) for √β<25. The curve AA represents average values of all data obtained here, which include the range of U
C/U
D=0-36, √β=0.3-400, u
D<100cm/sec., and U
C<110m/hr. For the large tip diameter (a=0.50cm), the data of au
Dρ
D/μ
D>1500 are omitted in Fig. 6, because they are higher than the curve as shown in Fig. 4 and Fig. 5. For comparison the data of Johnson and Bliss are also plotted in Fig. 6.
3) Flooding 
Although all of the flooding data are plotted near the right end of the curve AA in Fig. 6, the better correlation will be obtained if the exponents of (1+U
C/U
D) in the coordinates, 0.5 and 0.4, be replaced by 0.6 and 0.3, respectively, so far as the flooding phenomenon concerned. Thus, for the safe operation the value of (1+U
C/U
D)
0.3(1-a/D)
2ε should not be greater than 20%, and the value of (1+U
C/U
D)0.6(U
D/√ga) or (2.3/β
0.13)(1+U
C/U
D)
0.6 (U
D/√ga) should not be greater than 0.08.
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