The magnetization and demagnetization processes in the 11 types of Dy-free Nd-Fe-B sintered magnets based on the NEOMAX-50 type magnets were investigated using the step method that is our original method of measurements and analyses of minor loops with step by step increased maximum applied fields. With the decrease in average grain sizes (
DAVE), the single-domain grains (SDG) volume fraction increased and inversely that of the saturable multi-domain grains (SMDG) decreased, the changing behavior was monotonous. The dependence of coercivities on the
DAVE, however, showed clear change around
DAVE=3.0 μm, from the increase with decreasing
DAVE to the opposite relationship less than
DAVE ‹ 3.0 μm. We consider that the changing in the relationships should come from the ratios of the domain width (
WD) to the
DAVE, and conclude that the well cutting of magnetic interactions at the grain boundaries should realize the coercivity of
μ0H
C ≈ 2 T in fine grain size Dy-free samples.
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