1966 Volume 30 Issue 7 Pages 659-662
So called ambreinolal (IV), * a component of ambergris, was first synthesized by CrO3 oxidation of ambreinolol (III)* which was obtained from ambreinolide (II) by reduction with LiA1H4. Ambreinolol (III) was converted to the C17-saturated oxide (VII) in a good yield through the monotosylate (VIII) by treatment with p-toluenesulfonyl chloride in pyridine.
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