Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
Notes
Synthesis of Granulatimide Positional Analogues
Takuji Yoshida, Masakazu Nishiyachi, Nobuyuki Nakashima, Masayuki Murase, Eiichi Kotani
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Keywords: alkaloid, indole, maleimide, imidazole, Stille coupling reaction, synthesis
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2003 Volume 51 Issue 2 Pages 209-214

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Abstract
The Stille coupling reaction of the stannylindole 13 with the 5-iodoimidazole derivative 14 (or 27) in the presence of PdCl2(PPh3)2 gave the corresponding indole-imidazole coupling product 15 (or 28), thereby affording a synthetic approach to 10-methylgranulatimide (7), 15-methylgranulatimide (11), and 10, 15-dimethylgranulatimide (12), as well as 10-methylisogranulatimide B (5).
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© 2003 The Pharmaceutical Society of Japan
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