Facile Characterization of Polymer-Supported Reagents Using Cross Polarization Magic Angle Spinning Method in Solid State 13C-NMR

Kazuaki Shikii; Hiroko Seki; Kentaro Yamaguchi; Wannaporn Disadee; Toshiko Watanabe; Tsutomu Ishikawa

doi:10.1248/cpb.52.864

Chemical and Pharmaceutical Bulletin

Online ISSN : 1347-5223
Print ISSN : 0009-2363

Notes

Facile Characterization of Polymer-Supported Reagents Using Cross Polarization Magic Angle Spinning Method in Solid State ¹³C-NMR

Kazuaki Shikii, Hiroko Seki, Kentaro Yamaguchi, Wannaporn Disadee, Toshiko Watanabe, Tsutomu Ishikawa

Author information

Keywords: PS reagent, solid state NMR, cross polarization magic angle spinning, energy dispersive X-ray spectroscopy, PS-dimethylimidazolidinone

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Volume 52 (2004) Issue 7 Pages 864-865

DOI https://doi.org/10.1248/cpb.52.864

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Abstract

Polymer-supported (PS) reagents can be easily characterized using a cross polarization magic angle spinning method in solid state ¹³C-NMR. The technique was applied to the characterization of PS-dimethylimidazolidinone, analogue to potential heterogeneous dehydrating agent.

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