Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
Studies on Steroid Conjugates. II. Synthesis of 16-Epiestriol Monoglucuronides
TOSHIO NAMBARA, YASUHIKO MATSUKI, TOMOMI CHIBA
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1969 Volume 17 Issue 8 Pages 1636-1640

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Abstract
16-Epiestriol 16- and 17-monoglucuronides (XI, V) were prepared from 3-benzyloxy-17β-hydroxyestra-1, 3, 5 (10)-trien-16-one (I) employing Koenigs-Knorr reaction as shown in Chart 1. These synthetic glucuronides readily underwent hydrolysis with beef-liver β-glucuronidase preparation to furnish 16-epiestriol and free glucuronic acid.
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© The Pharmaceutical Society of Japan
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