Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
Radical Cycloaddition by Nickel(II) Complex-Catalyzed Electroreduction. A Method for Preparation of Pyrrolopyridine and Pyrrolopyrrole Derivatives
Shigeko OZAKI, Shizue MITOH, Hidenobu OHMORI
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Keywords: sequential radical reaction, indirect electroreduction, nickel(II) complex, cycloalkano[α]pyrrole, 1-(2-iodoethyl)pyrrole
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1996 Volume 44 Issue 11 Pages 2020-2024

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Abstract
Cycloalkano[α]pyrroles were obtained by reductive radical cycloaddition of 1-(2-iodoethyl)pyrrole and activated olefins or by cyclization of 1-(ω-iodoalkyl)pyrroles, through electroreduction of the iodides using nickel(II) complex as an electron-transfer catalyst.
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© The Pharmaceutical Society of Japan
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