Incorporation of a hydrophilic amide monomer into a one-step self-etch adhesive to increase dentin bond strength: Effect of application time

Abstract

The purpose was to evaluate the effect of a hydrophilic amide monomer on μTBS of one-step adhesive to dentin at different application times. Clearfil Universal Bond Quick (UBQ), experimental adhesive (UBQ_exp; same compositions as UBQ but hydrophilic amide monomer was replaced with 2-hydroxyethyl methacrylate), Clearfil SE ONE and Clearfil SE Bond were applied to midcoronal dentin prepared with 600-grit SiC at different application time (0, 10, 20 and 40 s). Water sorption (Wsp) and the ultimate tensile strength (UTS) of polymerized adhesives were also measured. UBQ showed significantly lower Wsp and higher UTS than UBQ_exp. At each application time, UBQ exhibited significantly higher μTBSs than UBQ_exp. UBQ showed the highest μTBS at 0 s application time among all the adhesives. When the application time was prolonged from 0 s to 10 s, only UBQ showed no significant difference. The hydrophilic amide monomer increased μTBS with reduction in Wsp and increase in the UTS and may allow a shortened application time.