Dental Materials Journal
Online ISSN : 1881-1361
Print ISSN : 0287-4547
ISSN-L : 0287-4547
Original Paper
Influence of primer contamination on the bonding interface of enamel pre-etched with phosphoric acid
Takaaki SATOToru NIKAIDOTomohiro TAKAGAKIYuta BABAMartina VICHEVAAyaka SATOJunji TAGAMI
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2021 Volume 40 Issue 5 Pages 1086-1093

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Abstract

In this study, the influence of primer contamination on enamel bonding was analyzed. Adper Scotchbond Multi-Purpose (SMP), CLEARFIL SE Bond 2 (SE2), Scotchbond Universal (SBU) Adhesive, and Scotchbond Etchant (35% phosphoric acid; PA) were used. Ground bovine enamels were divided into eight groups based on the bonding protocols. The bonding interfaces after an acid–base challenge were observed via scanning electron microscopy to determine the acid–base resistant zone (ABRZ). Moreover, the bonding interfaces after the nanoleakage challenge were analyzed via energy-dispersive X-ray spectroscopy. ABRZ was observed in all the samples except PA_ONLY (applied PA etching, No primer and No adhesive resin). The funnel-shaped erosion was detected only in X_SBU (applied SBU without PA etching). The nanoleakage test revealed silver patterns in some groups. The nanoleakage, i.e., the penetration of the silver ions, was detected in the groups wherein primer was applied on PA–pre-etched enamel.

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© 2021 The Japanese Society for Dental Materials and Devices
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