電気学会論文誌A(基礎・材料・共通部門誌)
Online ISSN : 1347-5533
Print ISSN : 0385-4205
ISSN-L : 0385-4205
ポリマーがいし外被の劣化診断手法(第1報)
試料の前処理法と各種分析技術
越野 幸広梅田 逸樹荒川 克己
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ジャーナル フリー

2000 年 120 巻 5 号 p. 657-664

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This paper describes pre-treatment and analytical method for determination of deterioration of silicone rubber housing for outdoor insulator. Washing with water and MIBK (Methyl-iso-butyl ketone) by ultrasonic washer was most effective to remove contaminant deposited on the surfaces of the housing. μ-FT-IR (Fourier transform infrared spectrophotometer equipped with infrared microscope) gave valuable information to determine the deterioration of the housing surfaces. It could make to analyze decreasing of ATH (ahnina tri-hydrate) in the silicone rubber specimens soaked in nitric acid, and surface oxidation of the specimens tested by fluorescent UV-condensation type weathering tester.
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