低温工学
Online ISSN : 1880-0408
Print ISSN : 0389-2441
ISSN-L : 0389-2441
液体ヘリウム用比熱測定装置
高田 義岡路 正博
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ジャーナル フリー

1978 年 13 巻 1 号 p. 27-34

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We designed a calorimeter for the liquid helium and constructed it. The calorimeter has a needle valve assembly which operates at the liquid helium temperature. The needle valve assembly enables one to seal the sample cavity and evacuate the filling tube. This excludes next troubles; the large heat leak due to the superfluid film flow, the change of the 3He mole fraction and the amount of the sample during the experiment. When this calorimeter is isolated thermally, it can be kept at extremely constant temperature by controlling the temperature of the surrounding liquid helium bath. The drift rate of temperature was less than 1.7×10-6K/hour. It corresponds to the heat leak of 0.5erg/min. This temperature stability and our temperature resolution. 1×10-7K, enable one to perform heat capacity measurements very near Tλ (superfluid transition temperature), 3×10-6K_??_|T-Tλ|<10-2K.
The drift rates of resistivity at Tλ were also examined on a carbon thermometer (Allen-Bradley 1/8W 47Ω) and a germanium thermometer (Scientific Instruments model NI). The indication of a germanium thermometer was found to be constant within experimental errors, but that of a carbon thermometer varied markedly. After cooling a carbon thermometer and keeping it at Tλ±0.1K for 40 hours, the drift rate of its indication was reduced to about 6×10-6K/hour.
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