燃料協会誌
Online ISSN : 2185-226X
Print ISSN : 0369-3775
ISSN-L : 0369-3775
熱重量法による石炭液化油の蒸留試験法
長谷川 義久吉田 忠成田 英夫前河 涌典
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1987 年 66 巻 10 号 p. 855-860

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A simple distillation method using conduction type thermogravimetric meter (TG) on coal-derived liquids was investigated.
It was found that under the following measuring conditions, this distillation method was good agreement with the standard distillation method (ASTM D-2892) which is used crude oil.
1) Thermoelectromotive force difference in thermocouples between the heat buffer cover and sample container (bias voltage): 300μV
2) Quantity of samples: 300-400mg It was also possible to measure the water content in coal-derived liquids with this method. The one-cycle measuring time required for the TG distillation method using a conduction type thermobalance was less than 90 minutes and this method was far quicker and easier than other methods. Furthermore, in terms of accuracy, it was considered that the method can com-pare well with the ASTM method.
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