軽金属
Online ISSN : 1880-8018
Print ISSN : 0451-5994
ISSN-L : 0451-5994
研究論文
低温における純アルミニウムのクリープ機構に対する純度の影響
松永 哲也佐藤 英一
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ジャーナル フリー

2014 年 64 巻 2 号 p. 42-48

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Creep tests were performed at less than 0.4 Tm (Tm is the melting temperature) for 99.999%, 99.57%, and 99.52% aluminum with several grain sizes in the range of 50–330 µm. These Al materials show remarkable creep behavior with an apparent activation energy (Q) of 30 kJ/mol, a stress exponent of 4, and a grain-size exponent of zero, and with a larger creep rate with increasing purity. These parameters resemble those of conventional dislocation creep, which is rate-controlled by the usual diffusion processes, except for the extra-low Q value. This means that a non-diffusional process affects the steady state deformation in this temperature region. Transmission electron microscopy revealed the development of a cell structure in the steady state and dislocations without any tangles in the cell interiors. Therefore, because the rate-controlling process could not occur inside of the cells, dislocation annihilation occurred through cross slip around the cell walls. According to these creep parameters and microstructural observations, the observed creep region is suggested to be a new creep region occurring through a non-diffusional process within the existing deformation mechanism map of Al at less than 0.4 Tm.
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© 2014 一般社団法人 軽金属学会
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