Comparison of the shear bond strength of composite resins with zirconia and titanium using different resin cements

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Purpose: The shear bond strength of conventional zirconia (3Y-TZP), translucent zirconia (5Y-PSZ), and titanium alloy (Ti6Al4V) thermocycled using different phosphate monomer resin cements were investigated.
Methods: In this study, 120 specimens of 3Y-TZP, 5Y-PSZ, and Ti6Al4V were cemented to nanocomposite resin cylinders using PANAVIA™ V5 and Rely X™ U200. The bond area and resin cement thickness were controlled as per ISO 29022:2013 and 4049:2009. Each resin cement group was used with/without the Clearfil ceramic primer plus. The shear bond strength of the 12 groups was statistically analyzed using two and one-way ANOVA to determine the properties of the different materials and resin cements (α = 0.05). The mode of failure was observed using scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS).
Results: The titanium alloy groups showed better shear bond strength than the zirconia groups (p < 0.05). PANAVIA™ V5 without primer showed significantly lower shear bond strength than other cements in zirconia and titanium alloy specimens (p < 0.05). Titanium alloy with Rely X™ U200 with a Clearfil ceramic primer plus showed the highest shear bond strength (6.37 ± 1.60 MPa). SEM images showed mixed failures in zirconia groups and cohesive failures in titanium alloy groups.
Conclusions: The titanium alloy showed better shear bond strength than zirconia when the Clearfil ceramic primer plus was used. The primer solution containing MDP and resin cement with phosphoric methacrylate ester showed similar shear bond strength with 3Y-TZP and 5Y-PSZ. The resin cement without phosphate monomers demonstrated the least shear bond strength.