MATERIALS TRANSACTIONS
Online ISSN : 1347-5320
Print ISSN : 1345-9678
ISSN-L : 1345-9678
Simultaneous Determination of the Composition and Size of Oxide Particles in Solid Materials by Laser Ablation-Inductively Coupled Plasma Mass Spectrometry
Andrey V. KarasevRyo Inoue
Author information
JOURNAL FREE ACCESS

2009 Volume 50 Issue 2 Pages 341-348

Details
Abstract
Laser ablation-inductively coupled plasma mass spectrometry (LA-ICP-MS) has been used for the determination of the composition and size of oxide particles consisting of SiO2, MnO, Al2O3, MgO and CaO on the surface of a glass or metal sample. The composition and size of multicomponent oxide particles such as MnO-SiO2, CaO-Al2O3 and CaO-Al2O3-MgO evaluated by LA-ICP-MS are compared with those obtained by chemical analysis and by SEM observation. It is confirmed that LA-ICP-MS method has prospects to be applied for quick and simultaneous measurement of the composition and size of particles on the surface of metals in steelmaking industry. The difference between the particle size determined by LA-ICP-MS and that by SEM ranges from 6 to 13% on an average in the range of dV=7∼40 μm.
Content from these authors
© 2009 The Japan Institute of Metals and Materials
Previous article Next article
feedback
Top