N,N-ジメチル-p-ニトロソアニリンの電解還元によるN,N-ジメチル-p-フェニレンジアミンの合成

抄録

N, N-Dimethyl-p-phenylenediamine was prepared in about 80% yield through the electroreduction of N, N-dimethyl-p-nitrosoaniline by 4.0 Fimol of electricity under a constant current density of 0.005 A/cm² in 10% H₂SO₄ aq. or 10% H₂SO₄ aq. -MeOH medium by using a stainless steel, carbon or platinum plate as a cathode electrode.