ビタミン
Online ISSN : 2424-080X
Print ISSN : 0006-386X
ビタミンB_1製品中の2-METHYL-4-AMINO-5-HYDROXYMETHYL PYRIMIDINE : (I) ビタミンB_1および関連化合物のPAPER PARTITION CHROMATOGRAPHY
小川 俊太郎西村 秀子
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ジャーナル フリー

1958 年 14 巻 p. 423-426

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OMP, a toxic decomposition product of thiamine can be clearly separated from other related compounds by paper partition chromatography using butanol・acetic acid・water (4 : 1 : 5) as developer and can be found located definitely under ultraviolet light (wave-length of 254mμ) as a dark image. Although semiquantitative experiment reveals that contamination of OMP or other impurities such as SB, TDS, B_1-thiazolone, Thiochrome, AMP or Th may not exceed 1% for ordinary crystalline thiamine salt, at least two unidentified substances having smaller or larger Rf value than thiamine appear on the cbromatogram. These substances show thiamine-like properties towards chemical reactions.
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© 1958 日本ビタミン学会

この記事はクリエイティブ・コモンズ [表示 - 非営利 - 改変禁止 4.0 国際]ライセンスの下に提供されています。
https://creativecommons.org/licenses/by-nc-nd/4.0/deed.ja
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