Synthesis and Crystal Structure of [RuCl(6-hydroxypicolinato)(2,2′;6′,2″-terpyridine)]·(N,N-dimethylformamide)

Yukitoshi NAKAMA; Takanori NISHIOKA; Takayuki NAKASONE; Eiji ASATO; Isamu KINOSHITA; Satoshi TAKARA

doi:10.2116/xraystruct.26.33

Part 4

Synthesis and Crystal Structure of [RuCl(6-hydroxypicolinato)(2,2′;6′,2″-terpyridine)]·(N,N-dimethylformamide)

Yukitoshi NAKAMA, Takanori NISHIOKA, Takayuki NAKASONE, Eiji ASATO, Isamu KINOSHITA, Satoshi TAKARA

著者情報

ジャーナルフリー
電子付録

2010 年 26 巻 p. 33-34

DOI https://doi.org/10.2116/xraystruct.26.33

詳細

抄録

The structure of [RuCl(6-hydroxypicolinato)(2,2′;6′,2″-terpyridine)]·(N,N-dimethylformamide) was determined by X-ray crystallography. The compound crystallized in a monoclinic system and was characterized thus: P2₁/c, a = 15.7325(19), b = 10.0621(10), c = 15.6422(19)Å, β = 105.112(3)°, Z = 4, V = 2390.6(5)Å³. The crystal structure was solved by the SIR97 direct method and refined by full-matrix least-squares on F² to final values of R1 = 0.1155 and wR2 = 0.1018 for all data.

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