Synthesis and Crystal Structure of a Benzoxazole Derivative: (E)-2-(6-Methylbenzoxazol-2-yl)-3-phenylacrylonitrile

Mohamed BELHOUCHET; Chiraz YOUSSEF; Hamed BEN AMMAR; Ridha BEN SALEM; Tahar MHIRI

doi:10.2116/xraystruct.28.3

Part 1

Synthesis and Crystal Structure of a Benzoxazole Derivative: (E)-2-(6-Methylbenzoxazol-2-yl)-3-phenylacrylonitrile

Mohamed BELHOUCHET, Chiraz YOUSSEF, Hamed BEN AMMAR, Ridha BEN SALEM, Tahar MHIRI

著者情報

ジャーナルフリー
電子付録

2012 年 28 巻 p. 3-4

DOI https://doi.org/10.2116/xraystruct.28.3

詳細

抄録

A benzoxazole derivative, (E)-2-(6-methylbenzoxazol-2-yl)-3-phenylacrylonitrile (abbreviated MBPA), with the formula C₁₇H₁₂N₂O was obtained by the Knovenegel reaction. This compound crystallizes in the monoclinic space group P2₁/c with the following cell parameters: a = 11.0508(8)Å; b = 12.0159(10)Å; c = 10.0074(9)Å; β = 94.761(5)°; V = 1324.25(19)Å³; Z = 2; R₁ = 0.052 and wR₂ = 0.142 for 2755 observed reflexions. The crystal structure of the synthesized compound was built by organic layers parallel to the [101] direction.

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