Part 5
Synthesis and Crystal Structure of 1,3-Bis(5-chloro-3-methoxysalicylideneamino)-2-propanol Trihydrate
2019 年 35 巻 p. 33-34
詳細
2019 年 35 巻 p. 33-34
The title compound, 1,3-bis(5-chloro-3-methoxysalicylideneamino)-2-propanol trihydrate, was synthesized and the crystal structure was determined by the single-crystal X-ray diffraction method at 90 K. It crystallizes in the monoclinic space group P2/c with a = 18.098(3)Å, b = 4.3275(8)Å, c = 14.572(3)Å, β = 104.283(3)°, V = 1106.0(3)Å3, Dx = 1.445 g/cm3, and Z = 2. The R1 [I > 2σ(I)] and wR2 (all data) values are 0.0734 and 0.2140, respectively, for all 2540 independent reflections. The molecule takes a bended structure at the central carbon atom with a dihedral angle between the two approximate planes of 74.71°.
