X-ray Structure Analysis Online
Online ISSN : 1883-3578
ISSN-L : 1883-3578
Part 2
Crystal Structure of Platinum and Rhodium Discrete Hexanuclear Complex with Polyethylene Glycol
Kazuhiro UEMURA
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2022 年 38 巻 p. 25-26

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The structure of [{Rh2II,II(O2CCH3)4}{Pt2II,II(acam)2(NH3)4}2(PF6)4·C24H48O12]n (acam = acetamidate) was determined via X-ray crystallography. The substance crystallizes in a triclinic system, and is described as follows: P-1, a = 10.8370(3), b = 11.4188(4), c = 19.4055(7)Å, α = 84.079(3)°, β = 89.031(3)°, γ = 62.366(3)°, Z = 2, V = 2114.77(13) Å3. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0620 and wR2 = 0.1126.

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© 2022 by The Japan Society for Analytical Chemistry
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