アルカロイド類のガスクロマトグラフィー : 第4報 若干のAconitum属アルカロイドーの分離
1968 年 88 巻 9 号 p. 1242-1244
詳細
1968 年 88 巻 9 号 p. 1242-1244
Separation of some Aconitum alkaloids by gas chromatography of trimethylsilyl ethers were attempted successively. The stationary liquid phases used were SE-30 (3%), OV-1 (5%), OV-17 (3%), and XE-60(3%). Retention times and chromatograms are shown in Table I and Figure 1 and 2 respectively. With a OV-17 column, kobusine and pseudo-kobusine were not well separated, and with a XE-60 column, in addition, benzoylaconine was not detected. The better chromatograms were obtained using a non-polar column (SE-30 or OV-1).
