Structural Analysis of Partially Acetylated Glycosides by Refocused-Decoupled Insensitive Nuclei Enhanced by Polarization Transfer (INEPT) Experiments: A Qualitative and Quantitative Method

Laurent Pouységu; Bernard De Jéso; Jean-Claude Lartigue; Michel Pétraud; Max Ratier

doi:10.1248/cpb.50.1114

Notes

Structural Analysis of Partially Acetylated Glycosides by Refocused-Decoupled Insensitive Nuclei Enhanced by Polarization Transfer (INEPT) Experiments: A Qualitative and Quantitative Method

Laurent Pouységu, Bernard De Jéso, Jean-Claude Lartigue, Michel Pétraud, Max Ratier

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Keywords: carbohydrate chemistry, enzymatic hydrolysis, ¹³C-NMR, refocused-decoupled INEPT, computer simulations, acetylated glycosides

JOURNAL FREE ACCESS

2002 Volume 50 Issue 8 Pages 1114-1117

DOI https://doi.org/10.1248/cpb.50.1114

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Abstract

The application of the refocused-decoupled INEPT pulse sequence in ¹³C-NMR spectroscopy allows, in conjonction with computer simulations, a straightforward editing of the spectra of a raw mixture of glycosidic compounds.

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