Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
A New Fluorometric Analysis of Dulcin using Sodium Nitrite. III. Structural Determination of the Fluorescent Compound by the Single Crystal X-Ray Diffraction Method
YOICHI IITAKASADAO UCHIYAMAZENZO TAMURA
Author information
JOURNAL FREE ACCESS

1972 Volume 20 Issue 6 Pages 1181-1185

Details
Abstract
The structure of the fluorescent compound (A) obtained from the reaction of dulcin and sodium nitrite was previously presumed to be 1, 3-bis (4-ethoxyphenyl)-5-tetrazolone. In this paper, (2-bromoethoxy) phenyl derivative (B) which has the same structural skeleton of compound A was synthesized and analized by the single crystal X-ray diffraction method to determine the structure more conclusively. The structure of compound B was discussed on the basis of the result of the two-dimensional analysis. The structure of the fluorescent compound A was consequently concluded as 1, 3-bis (4-ethoxyphenyl)-5-tetrazolone.
Content from these authors
© The Pharmaceutical Society of Japan
Previous article Next article
feedback
Top