Chemical and Pharmaceutical Bulletin
Online ISSN : 1347-5223
Print ISSN : 0009-2363
ISSN-L : 0009-2363
An Efficient One-Pot Method for the Large-Quantitative Produciton of Radiopharmaceutical Ligand : Diazadioximes
Hueisch-Jy DING, Ying-Fong HUANG, Cherng-Chyi TZENG, Si-Jung YEH, Li-Lan WEI
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Keywords: brain radiopharmaceutical ligand, one-pot method, diazadioxime, large-quantitative production
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2000 Volume 48 Issue 2 Pages 288-289

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Abstract
An efficient one-pot procedure for the preparation of diazadioxime was described. Treatment of ketooximes with alkyldiamine followed by NaBH4 by in dry ethanol afforded the correspponding d, l-diazadioximes in 56-74% yield without isolation of the intermediates.
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© The Pharmaceutical Society of Japan
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