日本水産学会誌
Online ISSN : 1349-998X
Print ISSN : 0021-5392
ISSN-L : 0021-5392
紅藻ツルツルより新ペプチド, L-citrullinyl-L-arginineの単離
宮沢 啓輔伊藤 啓二
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1974 年 40 巻 8 号 p. 815-818

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The methanolic extract of a red alga Grateloupia turuturu was found to contain a large amount of an unknown base. It was isolated by ionexchange resin column chromatography and shown to afford arginine, citrulline and ornithine on acid hydrolysis. Its DNP-derivative was obtained as needles and gave DNP-citrulline and arginine when hydrolyzed with acid. The behavior of this peptide coincided well with that of synthesized L-citrullinyl-L-arginine on paper chromatography with 4 different solvent systems. The DNP-derivatives prepared from the isolated and synthesized specimens showed good agreement in both IR spectrum and melting point.
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