Part 7
Crystal Structure of [Dihydrido-hexaphenylcarbodiphosphoran][chlorid][trichlorido-triphenylphosphino-platinat]
2021 年 37 巻 p. 33-34
詳細
2021 年 37 巻 p. 33-34
The crystal structure of the salt [dihydrido-hexaphenylcarbodiphosphoran][chlorid][trichlorido-triphenylphosphino-platinat] was determined by X-ray crystallography. The title compound crystallizes in the monoclinic space group with the cell parameters a = 38.858(3)Å, b = 10.851(1)Å, c = 27.666(2)Å, α = 90°, β = 109.07(1)°, γ = 90°, V = 11025(2)Å3, Z = 8. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F2 to final values of R1 = 0.0771 and wR2 (all data)= 0.1732, T = 100(2)K.
