YAKUGAKU ZASSHI
Online ISSN : 1347-5231
Print ISSN : 0031-6903
ISSN-L : 0031-6903
Synthesis of p-Ethylsulfonylbenzaldehyde Thiosemicarbazone
Haruki Satoh
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1951 Volume 71 Issue 12 Pages 1364-1366

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Abstract
Of the thiosemicarbazones of benzaldehyde with substituent in the para position which were said to be as effective as Tibione, p-ethylsulfonylbenzaldehyde thiosemicarbazone was prepared by the condensation of thiosemicarbazide and ethylsulfonylbenzaldehyde. This aldehyde was obtained from the corresponding methyl derivative, i.e. p-tolylethyl sulfone, by its oxidation with chromic and sulfuric acids in acetic anhydride to aldehyde diacetate, followed by hydrolysis.
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