A Laboratory vacuum furnace has been constructed in order to study how to prepare the oxygen-free metals and alloys, and to develop the metallic materials used in electronic industry or any other fields which need them durable at high temperature. In this unit, melting due to either of induction and arc or resistance heating can be carried out in high vacuum or an atmosphere of hydrogen or other inert gas. And, annealing or other heat treatment in a vacuum or a controlled atmosphere and degassing of graphite or refractories are also capable in this vacuum furnace.
The chamber of the furnace has a volume of about 120 liters, and has coaxial leads which lead high frequency or other electric current for heating into the chamber, and a melt is poured by rotating the coaxial leads.
The chamber is evacuated by a 10 inches oil diffusion pump, and the pressure in it is in a range of 10
-5mmHg when a pouring of metal is ended. Induction heating is carried out by a vacuum-tube generator which has the maximum output of about 40 kilowatts and the ordinary frequency of 15 ki kilocycles per second, and the melting or casting capacity is usually about 5 lbs for nickel in case of induction melting.
On apparatus for determination of oxygen or other gases in metals has been also prepared as a belongings of this vacuum furnace at the same time. This is a modification of those which have been prepared at several laboratories in America and Europe. Like the general type of the apparatus for vacuum fusion gas analysis, it consists of three sections of gassware : a small vacuum fusion furnace, a section for extraction and measurement, and one for analysis of gases extracted. And in any section, none of, rubber, grease or oil is used, and all pumps and cutoffs are mercury ones.
The vacuum fusion furnace is a Guldner-type, and a graphite crucible used in it can be degassed at about 2500°C by induction heating from the outside of a borosilicate glass tube.
View full abstract