衛生化学
Print ISSN : 0013-273X
抗酸化剤に関する研究(I) : 薄層クロマトグラフィーによる抗酸化剤の分離, 定性およびBHAの定量について
呉地 伝夫荻野 喜文
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ジャーナル フリー

1964 年 10 巻 4 号 p. 261-265

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Separation analysis of nine kinds of antioxidants and quantitative determination of BHA were investigated by means of silica gel thin-layer chromatography. Benzene-ether (1 : 2) and chloroform-ether (1 : 3) were found as suitable solvent systems for two dimensional chromatography, and the minimum amount for identification was 1 μg per ml. For determination of BHA, 2, 6-dichloroquinone 4-chlorimide were used as a color reagent and the colored spot was scraped off from the plate, extracted with ether and determined spectrophotometrically.
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© 社団法人 日本薬学会
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