水産物に添加された酸化防止剤の定量に関する研究-II BHA, BHTの定量に対する水蒸気蒸留法の適用について

外山 健三; 鈴木 幹夫

doi:10.2331/suisan.27.1084

水産物に添加された酸化防止剤の定量に関する研究-II

BHA, BHTの定量に対する水蒸気蒸留法の適用について

外山健三, 鈴木幹夫

著者情報

ジャーナルフリー

1961 年 27 巻 12 号 p. 1084-1087

DOI https://doi.org/10.2331/suisan.27.1084

詳細

発行日: 1961/12/25 受付日: - J-STAGE公開日: 2008/02/29 受理日: 1961/10/13 早期公開日: - 改訂日: -
訂正情報
訂正日: 2008/02/29 訂正理由: - 訂正箇所: 論文抄録訂正内容: Wrong : Seeking a method of unequivocally determining the BHA and BHT added to the marine products, the steam-distillation method (presented by ANGLIN et al.⁴⁾) was tentatively applied to the estimation of antioxidants in the extracts obtained by Soxhlet extraction from salted-and-dried saury, the following results being obtained.
By the steam-distillation method, the separation of the antioxidants can be completed far more rapidly than by the solvent-extraction method¹⁾, and estimation of BHA is carried out without any trouble, owing to the specific reactivity of 2, 6-dichloroquinonechloroimide (2, 6-D) reagent upon BHA. This method, however, is not suitable for thereby estimating BHT, since the 2, 2′-dipyridyl (2, 2′-DP) reagent reacts on some contaminations coming in the distillates, leading often to ambiguous results just like the case of solvent extracts descrived in the preceeding paper¹⁾.
Right : Seeking a method of unequivocally determining the BHA and BHT added to the marine products, the steam-distillation method (presented by ANGLIN et al.⁴⁾) was tentatively applied to the estimation of antioxidants in the extracts obtained by Soxhlet extraction from salted-and-dried saury, the following results being obtained.
By the steam-distillation method, the separation of the antioxidants can be completed far more rapidly than by the solvent-extraction method¹⁾, and estimation of BHA is carried out without any trouble, owing to the specific reactivity of 2, 6-dichloroquinonechloroimide (2, 6-D) reagent upon BHA. This method, however, is not suitable for thereby estimating BHT, since the 2, 2'-dipyridyl (2, 2'-DP) reagent reacts on some contaminations coming in the distillates, leading often to ambiguous results just like the case of solvent extracts descrived in the preceeding paper¹⁾.

訂正日: 2008/02/29 訂正理由: - 訂正箇所: PDFファイル訂正内容: -

抄録

Seeking a method of unequivocally determining the BHA and BHT added to the marine products, the steam-distillation method (presented by ANGLIN et al.⁴⁾) was tentatively applied to the estimation of antioxidants in the extracts obtained by Soxhlet extraction from salted-and-dried saury, the following results being obtained.
By the steam-distillation method, the separation of the antioxidants can be completed far more rapidly than by the solvent-extraction method¹⁾, and estimation of BHA is carried out without any trouble, owing to the specific reactivity of 2, 6-dichloroquinonechloroimide (2, 6-D) reagent upon BHA. This method, however, is not suitable for thereby estimating BHT, since the 2, 2'-dipyridyl (2, 2'-DP) reagent reacts on some contaminations coming in the distillates, leading often to ambiguous results just like the case of solvent extracts descrived in the preceeding paper¹⁾.

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