オリゴ糖の1,6-アンヒドロ誘導体の13C Nuclear Magnetic Resonanceスペクトル

松田 秀人; 手島 節三

doi:10.1248/yakushi1947.101.9_814

^<13>C Nuclear Magnetic Resonance Spectra of 1, 6-Anhydro Derivatives of Oligosaccharides

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Keywords: ^<13>C NMR proton off-resonance decoupling, one bond carbon-proton coupling constant, glycosidation shift, lactosan, maltosan, cellobiosan, 1, 6-anhydroaltrosylglucose, 1, 6-anhydro-idosylglucose, 1, 6-anhydro-trisaccharides

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1981 Volume 101 Issue 9 Pages 814-821

DOI https://doi.org/10.1248/yakushi1947.101.9_814

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Abstract

The ¹³C nuclear magnetic resonance spectral data of 16 kinds of free and substituted 1, 6-anhydro-β-derivatives of reducing disaccharides and trisaccharides in D₂O or pyridine-d₅ were presented, and their applications to structural analysis were discussed.

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