Food Science and Technology Research
Online ISSN : 1881-3984
Print ISSN : 1344-6606
ISSN-L : 1344-6606
Notes
Analysis of Sudan I in Food by QuEChERS Combined with Ultrasound-assisted Dispersive Liquid-liquid Microextraction with Solidification of Floating Organic Drop (UADLLME-SFO) Prior to HPLC-PAD
Xiran HeYonghong ChenHuawen LiTangbin ZouMingyuan HuangHuabin LiEnqin Xia
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2015 Volume 21 Issue 5 Pages 659-664

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Abstract

A convenient and environmentally friendly method was developed for extraction and enrich of Sudan I from tomato sauce and chilli products. The method is based on an ultrasound-assisted dispersive liquid-liquid microextraction with solidification of floating organic drop (UADLLME-SFO) after a preliminary QuEChERS procedure, which was followed by high performance liquid chromatography with photodiode array detection (HPLC-PAD). The several parameters involved in the UADLLME-SFO step was optimized. The optimal variables obtained were 30 µL of 1-dodecanol as the extraction solvent, 1.0 mL of acetone as disperse solvent, ultrasonic irritation for 15 min, and no salt addition. Under the optimum conditions, the limit of detection for Sudan I was as low as 1.5 µg kg−1. The recoveries obtained was between 79% and 92% (RSD, 4.8% – 7.1%, n = 7). The proposed method was successfully applied to the determination of Sudan I in four kinds of real samples.

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© 2015 by Japanese Society for Food Science and Technology
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