衛生化学
Print ISSN : 0013-273X
ヒト血液中からの農薬カルタップの抽出
三井 利幸藤村 義和
著者情報
ジャーナル フリー

1986 年 32 巻 4 号 p. 305-307

詳細
抄録
The selection of best solvent for extracting cartap from human blood was examined. The experimental procedures were as follows ; One ml of blood sample was added to 0.5 ml of 8% sodium hydroxide solution in a 15 ml test tube. The sample was extracted with 5 ml of cyclohexane by shaking for 3 min, and centrifuged at 3000 rpm for 2 min. The cartap extracted with cyclohexane was derivatized by reacting with 3, 4-dimethyl benzyl chloride. The 3, 4-dimethyl benzyl derivative of cartap was spectrophotometrically measured by using tropaeoline OO as an ion-associating reagent. For the extraction of cartap from blood sample no interference could be observed with the compounds, such as Fe (III), Cu (II), glycine, L-phenylalanine, urea, glucose, lactose.
著者関連情報
© 社団法人 日本薬学会
前の記事 次の記事
feedback
Top