油化学
Online ISSN : 1884-2003
ISSN-L : 0513-398X
熱伝導度型検出器をそなえたガスクロマトグラフによる脂肪酸組成の分析における補正係数の検討
渡辺 昭一郎中里 敏桑山 英夫笹本 幸弘白石 振作清野 肇永井 敏雄根岸 正明早野 茂夫
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ジャーナル フリー

1973 年 22 巻 2 号 p. 102-105

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Collaborative analyses were carried out to examine the effect of application of the correction factors on the determination of fatty acid composition by gas chromatograph with thermal conductivity detector. The appropriate use of the correction factors gave a good result, that is, the corrected value approached closely to the known values and the interlaboratory scattering was considerably decreased. It was observed that the correction factor was affected by the operating conditions and the fatty acid composition of the reference mixture as well as by the number of carbon atoms in the methyl ester. Accordingly, for the precise determination it is recommended to apply the correction factors which have been determined not only by analysing a reference mixture having a similar composition to that of an unknown but by using the same instrument under the same operating conditions as those for the analysis of the unknown.
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