The determination procedure for extremely low-level radio-iodine (
131I) in milk ( (23) × 10
-9 μCi/m
l) which corresponds to 15 mrem/yr of exposure dose for thyroid of a critical person (
i.e. a baby) were published recently by both United States Atomic Energy Com-mission and Battelle Pacific Northwest Laboratories. However, error of determination, lower limit of detection and time required for preconcentration and radiation counting were not shown. Therefore we examined these conditions for those two kinds of methods to know whether they are useful for practical performance or not.
(1) Recovery of iodine in milk was about 7075 % in both methods.
(2) Lower limit of detection of 131I in milk was 6.7 x 10
-11 μCi/m
l with 30.4% of CV for counting. The determination conditions are : (1) sample volume 4
l, (2) counting time 1, 000 min (16 2/3 hr), (3) iodine recovery 70 (4) efficiency of β-ray counting 30 %, background counting 0.8 cpm.
(3) In case of two-sample treatment in parallel, it took about 1.52 days for preconcentration procedure, and about 45 days for over-all determination.
(4) From the result mentioned above, it was clarified that extremely low-level radioiodine in milk which corresponds to 15 mrem/yr could be practically carried out by the both methods with experimental conditions mentioned in (2).
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