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44th Petroleum-Petrochemical Symposium of JPI (Asahikawa)

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Special lecture

What we show our guests are the greatness of animal life

Gen Bando

Pages 1-
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_1

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Polymer, oligomer

Synthesis of (imido)vanadium-alkylidene complexes and their use as catalysts for ring-opening metathesis polymerization of cyclic olefins

Xiaohua Hou, Akiko Inagaki, Kotohiro Nomura

Session ID: 1A01
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_2

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In this presentation, we wish to present our explored results concerning syntehsis of (imido)vanadium-alkylidene complexes and their use in catalysts for ring-opening metathesis polymerization of cyclic olefins especially norbornene derivatives.

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Design of homogeneous Phillips type catalyst by silsequoxane support

Yanning Zeng, Toshiaki Taniike, Minoru Terano

Session ID: 1A02
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_3

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The Phillips catalyst comprising Cr active species and silica support is responsible for the commercial production of high-density polyethylene (HDPE). However, the active-site structure and its relationship with polymer properties are still unclear, because of a great extent of surface heterogeneity. Polyhedral oligomeric silsequioxane (POSS) is regarded as a model silica, which can represent different surface silanol groups by various POSS cages and hydroxyl groups. In this study, we synthesized homogeneous Phillips catalysts using POSS. Catalyst characterization indicated that the Cr(III) precursor was reacted with two hydroxyl groups to bear (Me₃Si)₂CH-Cr(-O-Si-)₂ structures for both catalysts, remained one hydroxyl group in Cr(III)/POSS-3OH.

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Ring-opening metathesis polymerization of cyclic olefins by organo-vanadium catalysts

Yuuki Ootaka, Akiko Inagaki, Kotohiro Nomura

Session ID: 1A03
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_4

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Precise synthesis of star/ball shape polymers by living ring-opening metathesis polymerization (ROMP)

Kazuya Morishita, Akiko Inagaki, Kotohiro Nomura

Session ID: 1A04
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_5

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We wish to present our explored results concerning precise synthesis of star/ball shape polymers by living ring-opening metathesis polymerization of norbornenes using molybdenum-alkylidene catalysts.

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Fluid catalytic cracking reaction of polyethylene – Study of active species of iron-based catalyst –

Kenta Takehara, Kazuki Otani, Takeru Hotta, Katsuhiko Takagi, Noriyasu ...

Session ID: 1A05
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_6

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Industrial production of dicyclopentadiene resin by reaction injection molding using novel ruthenium catalyst.

Michiru Kamada, Toshiyuki Oshiki

Session ID: 1A06
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_7

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Dicyclopantadiene is C5 fraction of naphtha and a versatile monomer for ring opening metathesis polymerization (ROMP). Reaction injection molding of DCP (DCP-RIM) via ROMP is one of the most effective process to produce useful molding products in industry. Ruthenium based metathesis catalysts are well known to show excellent reactivity for ROMP of DCP, but it was difficult to apply to DCP-RIM process. We succeeded in the preparation of a high performance ruthenium catalyst for DCP-RIM in large scale.

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Control of molecular weight and its distribution in propene polymerization with ansa-(fluorenylamido)dimethyltitanium-metylaluminoxane/SiO₂ catalyst

Tomoyasu Kawahara, Taiki Tabuchi, Ryo Tanaka, Yuushou Nakayama, Takesh ...

Session ID: 1A07
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_8

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The use of SiO₂-supported MAO is the simplest supporting method of single-site catalysts. In this paper, we conducted propene polymerization with a Ti-based catalyst activated by several SiO₂-supported MAO and investigated the effects of polymerization conditions and the addition of R₃Al/SiO₂ on the molecular weight and its distribution of the polymer obtained.

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Polymer, oligomer-Invited lecture

Control of polymer structure using light

Tamaki Nakano

Session ID: 1A08
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_9

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Chiral structural regulation to polymers and small molecules was achieved using circularly polarized light as chiraliy sourse. First, a preferred-handed helical conformation was induced to main-chain conjugated polymers by this method. Second, the scope was expanded to vinyl polymers and related small molecules.

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Polymer, oligomer

The investigation of structure performance relationship of dialkoxysilane in the initial stage of propylene polymerization in the absence/presence of internal donors

Supawadee Poonpong, Toshiaki Taniike, Minoru Terano

Session ID: 1A09
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_10

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Various types pf alkoxysilane have been used as an external donor in propylene polymerization with MgCl2-supported Ziegler-Natta catalyst. This study was to investigate the structure-performance relationship in the level of active sites by stopped-flow polymerization combined with temperature rising elution fractionation (TREF) and density functional theory (DFT) calculations in terms of catalyst activity and stereoregularity. It was clarified that the bulkiness of hydrocarbon groups could not only explain the resulted catalyst performance. The conformation detail of hydrocarbon groups around active sites is also important. In the absence of internal donor, dicyclopentyldimethoxysilane (DCPDMS) gave the highest catalyst activity and stereospecificity which corresponds to the information of electronic and steric effects from DFT calculations. The further results from the internal donor-contained catalyst will help us for the better understanding of the alkoxysilane effects which applicable to the industrial aspects.

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Ethylene/1-hexene co-polymerization with bridged bis-indenyl metallocene catalysts

Tsutomu Sakuragi, Kouji Itagaki, Tomohiko Satou, Hiroyuki Shimizu, Hid ...

Session ID: 1A10
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_11

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Ethylene oligomerization catalyzed by bis(imino)pyridinecobalt(II) complexes immobilized in fluorotetrasilicic mica interlayer.

Shun Ishikawa, Kazuhiro Yamamoto, Tsutomu Sakuragi, Masaaki Ohshima, S ...

Session ID: 1A11
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_12

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Separation

Separation of n-alkanes with MFI-type zeolite membrane

Motomu Sakai, Takuya Kaneko, Masahiko Matsukata

Session ID: 1A12
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_13

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Silicalite-1, a pure silica MFI-type zeolite, membrane was prepared on a tubular a-alumina support by a secondary growth method. Separation of n-alkane from a mixture of hydrocarbons was carried out by using silicalite-1 membrane. We report the permeation and separation properties for n-alkanes having different carbon numbers.

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Control of pore structure of SPPO carbon membranes for hydrgen separaion from organic chemical hydrides

Miki Yoshimune, Kenji Haraya, Satoshi Furuta, Yuichiro Hirano, Hideshi ...

Session ID: 1A13
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_14

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Gas phase esterification in zeolite membrane reactor

Jun Ishida, Yuhei Kikuchi, Takafumi Sato, Naotsugu Itoh

Session ID: 1A14
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_15

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Study on effective coagulation of oil in polymar flood oilfield produced water

Keisuke Kojima, Masaharu Tasaki, Kazuo Okamura, Sueyoshi Mark, Al-Maam ...

Session ID: 1A15
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_16

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Pilot trials for oilfield produced water treatment in Oman

Masaharu Tasaki, Keisuke Kojima, Kazuo Okamura, Mark Sueyoshi, Rashid ...

Session ID: 1A16
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_17

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Hydrogenation, dehydrogenation

Exploration of catalysts for simple dehydrogenation of 1-butene

Masahiko Matsukata, Kota Yamagami, Naoki Kanaya

Session ID: 2A01
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_18

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We explored catalysts for the simple dehydrogenation of 1-butene to 1,3-butadiene. 4 types of zeolite and 5 sorts of metal oxide were tested as support by loading of 0.4 wt% Pt. Then, Cr, Ce, Fe were tested as additive on the selected support. Pt was also 0.4 wt%. The loading amount of additive was optimized. We discussed the reasons of a high yield and selectivity to 1,3-butadiene over the catalyst developed on the basis of the results of NH₃-TPD, TPO, XRD.

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Oxidative dehydrogenation of n-C4 to butadiene over VMgO catalysts

Michiko Takasaki, Norihito Chiyoda, Soji Yamaguchi, Masaki Shimamura, ...

Session ID: 2A02
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_19

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Methylation of amines with carbon dioxide and hydrogen by supported Pt catalyst

Kenichi Shimizu, Kenichi Kon

Session ID: 2A03
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_20

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hydrogen transfer hydrogenation from decahydronaphthalene to naphthalene with platinum catalyst

Keisuke Otobe, Hiroshi Yamada, Tomohiko Tagawa

Session ID: 2A04
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_21

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Direct synthesis of heterocycles by dehydrogenative coupling of diamines and alcohols or aldehydes by supported Pt catalysts

Chandan Chaudhari, S. M. A. Hakim Siddiki, Kenichi Shimizu

Session ID: 2A05
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_22

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This study shows the synthesis of benzimidazoles and quinazolines under additive-free and acceptor-free conditions from alcohols or aldehydes with diamines using supported Pt catalysts.

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Supported Pt catalyst for dehydrogenative self-coupling of primary alcohols to esters

Sondomoyee Konika Moromi, S. M. A. Hakim Siddiki, Kenichi Shimizu

Session ID: 2A06
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_23

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Hydrogenation of olefin catalyzed organosilane-modified zirconia

Takahiro Nishiharaguchi, Hirotaka Inagaki, Hirofumi Yamada, Yuzo Imiz ...

Session ID: 2A07
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_24

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Additive effect of base component on CO₂ methanation activity of supported Ni catalysts

Yuji Tsuda, Takeou Okanishi, Hiroki Muroyama, Toshiaki Matsui, Koichi ...

Session ID: 2A08
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_25

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Development of metal-honeycomb-type Ni-based catalyst for transforming CO₂ to methane resource

Kotaro Hayakawa , Katsunori Murabayashi , Ryo Watanabe , Choji Fukuhar ...

Session ID: 2A09
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_26

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Desulfurization

Direct decomposition of methanethiol over metal oxide catalysts

Takashi Mukoyama, Naohiro Shimoda, Shigeo Satokawa

Session ID: 2A10
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_27

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Low temperature synthesis of Al₂O₃-supported noble metal phosphide catalyst for hydrodesulfurization

Yuki Matsukura, Ayaka Sawada, Yasuharu Kanda, Masatoshi Sugioka, Yoshi ...

Session ID: 2A11
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_28

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Detailed analysis of catalyst and feed oil for improvement of gas oil hydrodesulfurization process

Nobuharu Kimura, Yoshimu Iwanami, Shouzaburou Konishi, Ryutaro Koide, ...

Session ID: 2A12
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_29

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Measurement of diffusivity of naphtha related chemicals in coked H-ZSM-5 pores

Junichi Nishimura, Ryouta Ohnaka, Yuta Nakasaka, Teruoki Tago, Takao M ...

Session ID: 2A13
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_30

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Lubricants-Invited lecture

Corrosion of pure Al and Al alloys in aqueous solutions and alcohol

Hideaki Takahashi

Session ID: 2A14
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_31

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Lubricants

The effects of MoDTC and co-existing metal-based detergents on wear behavior of aluminum alloy in lubricating oil

Masahiro Morikane, Tatsuro Amano, Hiroto Turuo, Toshiaki Wakabayashi, ...

Session ID: 2A15
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_32

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Influence of thickeners on grease decomposition by nascent metal surface

Tomoya Ueta, Kenji Utsumi, Kyoji Kondo, Toshiaki Wakabayashi, Yasuha T ...

Session ID: 2A16
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_33

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In situ observation of molecular interaction of lubricant components at EHL contact

Koji Takiwatari, Shin-ya Sato, Hidetaka Nanao, Shigeyuki Mori

Session ID: 2A17
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_34

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Lubrication properties are closely dependent on the lubricant viscosity which is altered by high pressure and shearing at EHL contacts. The concentration and structure of lubricant oil at EHL contacts were observed with a micro-FTIR and the molecular interaction between lubricant components were characterized in order to understand lubricating property of the oil.

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In situ observation of thickener concentration of semi-solid lubricants by a micro infrared spectroscopy

Yasushi Hoshi, Koji Takiwatari, Ryusuke Sasaki, Hidetaka Nanao, Shigey ...

Session ID: 2A18
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_35

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Effect of base oil of urea grease on traction property under rolling contact

Hiroshi Komiya, Yuriko Ikeda, Hiroki Iwamatsu, Masashi Mitsuoka

Session ID: 2A19
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_36

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Frictional properties of high viscosity compound formulated oil

Kazuo Tagawa, Masayoshi Muraki

Session ID: 2A20
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_37

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Antioxidant action of sulfurized fatty acid ester

Kazuhiro Yagishita, Toshio Yoshida

Session ID: 2A21
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_38

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Lubricant technology in automatic transmissions

Keiichi Narita, Masato Yokomizo

Session ID: 2A22
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_39

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Automatic transmissions are divided into Step type AT (AT) and Continuously Variable Transmission (CVT). Lubricants used for AT and CVT are defined as ATF and CVTF. For the improvement of fuel efficient by lubricants, lower viscosity type ATF is useful because of reducing agitation loss in transmissions. It is also important to keep fatigue life performance in gear and bearing components in spite of the use of lower viscosity ATF. A sort of viscosity index improver (VII) would improve film thickness under the EHD lubrication condition. The performance requirement of CVT is to improve the metal-metal friction coefficient between the belt and pulley in the CVT and be compatible for wet clutch system. Lubricant additive formulation would give a great impact for these performances and the friction properties may depend on the properties of tribofilm (morphology and compositions).

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Evaluation of tribological property for hydraulic fluid by roller on disk test(Part3)

Yukiko Naka, Masakazu Otsuka, Hiroshi Kosodo, Masayuki Mitsui

Session ID: 2A23
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_40

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C1 chemistry

Synthesis of lower olefins from synthesis gas over iron catalyst

Kazuki Komiyama, Kenji Asami

Session ID: 1B01
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_41

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Crystal size control of SAPO-34 and its catalytic activity in olefin synthesis

Shinya Amano, Katsutoshi Yamamoto

Session ID: 1B02
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_42

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Selective synthesis of gasoline-ranged hydrocarbons from syngas over hybrid catalyst consisting of metal-loaded ZSM-5 coupled with copper-zinc oxid

Manami Yamawaki, Ting Ma, Kazusa Terasaka, Hiroyuki Imai, Xiaohong Li

Session ID: 1B03
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_43

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Effect of carbon dioxide and water in the reactant gas for dimethyl ether direct synthesis from syngas

Kaoru Takeishi, Yutarou Wagatsuma

Session ID: 1B04
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_44

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Fischer-Tropsch synthesis over iron catalyst supported on ozone-treated active carbon

Yusuke Kawahara, Kazuki Komiyama, Kenji Asami

Session ID: 1B05
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_45

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Phosgene-free synthesis of aromatic urethane from carbon dioxide

Jun-Chul Choi, Haoyu Yuan, Shun-ya Onozawa, Norihisa Fukaya, Hiroyuki ...

Session ID: 1B06
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_46

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We developed the environmentally benign synthetic method of aromatic urethane from amine and carbon dioxide without toxic and corrosive phosgene. Specifically, we have succeeded in the reaction of aniline and tin alkoxide in the presence of carbon dioxide (5 MPa) gave the corresponding aromatic urethane in the yields up to 80%.

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Environmental catalysts

Photocatalysis of lead oxide on decomposition of phenol

Kanta Chinomi, Takeshi Kubota, Kohji Omata

Session ID: 1B07
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_47

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Methane oxidation over palladium catalyst supported on mesoporous ZrO₂ including sulfate ions

Kenji Takamura, Masatomo Hattori, Masaaki Haneda

Session ID: 1B08
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_48

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Oxidative coupling of methane over supported polyoxometalate catalysts in an electric field

Shuhei Ogo, Kei Sugiura, Tomohiro Yabe, Yasushi Sekine

Session ID: 1B09
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_49

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Selective catalytic reduction of NO with hydrocarbons – Activity of each elementary reaction of BaZrO3-based catalyst –

Kenta Suzuki, Akitsuna Miyamoto, Tomomi Kusano, Noriyasu Okazaki

Session ID: 1B10
Published: 2014
Released on J-STAGE: December 16, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014f.0_50

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