Proceeding of Annual/Fall Meetings of the Japan Petroleum Institute

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63rd R&D Symposium of Jpn. Petrol. Inst.

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[Special Lecture]

Frontiers of energy-environmental policy in Japan

Kenji Yamaji

Session ID: 1S01
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_1

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Award Lectures

[Award Lecture-The Japan Petroleum Institute Award for Technological Progress]

Development and commerciallization of zinc and phosphorus modified NiMo catalysts for residue hydrodesulfurization

Nobumasa Nakajima, Yoshihiro Seriguchi, Mutsumi Kato, Motoki Yoshinari ...

Session ID: 1S02
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_2

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[Award Lecture-The Japan Petroleum Institute Award Distinguished Papers]

Effect of Sn addition of n-butane dehydrogenation over supported Pt catalysts

Iori Kikuchi, Masaaki Ohshima, Hideki Kurokawa, Hiroshi Miura

Session ID: 1S03
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_3

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Effect of fuel composition on vaporization behavior in gasoline engines

Koji Oyama, Gen Shibata, Seiichi Nakano, Tohru Isoda

Session ID: 1S04
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_4

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[Award Lecture-The Japan Petroleum Institute Award]

Development and commercialization of methyl methacrylate production technology by gold-nickel oxide nanoparticle catalysts with a core-shell structure

Ken Suzuki, Tatsuo Yamaguchi, Hideaki Goto, Seiichiro Yamane, Kohki Ad ...

Session ID: 1S05
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_5

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Aerobic oxidative esterification of methacrolein in methanol to methyl methacrylate (MMA) proceeds with high efficiency in the presence of molecular oxygen, on supported gold–nickel oxide (Au–NiO_x) nanoparticle catalysts. The method is environmentally benign because it requires only molecular oxygen as the terminal oxidant and gives water as the side product. The Au–NiO_x nanoparticles have a core-shell structure, with the Au nanoparticles at the core and the surface covered by highly oxidized NiO_x. The practical applicability of this catalytic system was verified in a 100,000 ton/year MMA production plant. This process confirmed the high selectivity, high activity, and long life of the Au–NiO_x catalyst. This catalyst would help in saving energy and resources, in addition to being highly economical.

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Development of simultaneous catalytic reduction system for nitrogen oxides and particulate mattter with diesel fuel

Shinya Sato, Yoshihiro Funayama, Takatoshi Furukawa, Mori Ishii, Masak ...

Session ID: 1S06
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_6

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Development of mixed oxide catalyst materials for solid oxide fule cells, combustion, and reforming

Koichi Eguchi

Session ID: 1S07
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_7

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[Regular Presentations]

PM oxidation using Ag supported ceria-based catalysts

Yusuke Okai, Junya Ohyama, Koji Omata, Atsushi Satsuma

Session ID: 1A01
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_8

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For clean diesel vehicles, effective oxidation of particulate matter (PM) at low temperatures is strongly required. In this study, carbon oxidation using ceria-based mixed metal oxides examined, and the effect of oxygen storage capacity (OSC) was discussed. When Mn and Ca are loaded to ceria, the oxidation temperature was lowered, and the promotion effect was correlated to the increase in OSC. Further loading of Ag promoted the carbon oxidation, and the maximum oxidation peak was lowered below 300 degree C.

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Preparation of ceria for three-way catalyst with high activity by non-linear regression models

Teppei Kihara, Takeshi Kubota, Kohji Omata

Session ID: 1A02
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_9

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Effect of preparation conditions on the acid catalytic properties of protonated titanate nanotubes

Masaaki Kitano, Kiyotaka Nakajima, Hisayoshi Kobayashi, Michikazu Hara

Session ID: 1A03
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_10

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The effect of hydrothermal treatment on the morphological and acid catalytic properties of titanate nanotubes was examined. Anatase nanoparticles were converted into titanate nanotubes and layered titanate nanorods according to the heating temperature used durign hydrothermal treatment. FT-IR measurement revealed that both Lewis and Bronsted acid sites are formed after hydrothermal treatment at temperatures higher than 323 K. Titanate nanotubes prepared at 423 K exhibited the highest catalytic activity for alkylation reaction.

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Acidic properties of H₄SiW₁₂O₄₀ supported on TiO₂ and Al₂O₃

Yuichi Kamiya, Yuichi Miyagi

Session ID: 1A04
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_11

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Mechanochemical and chemical modifications giving nano-sized ZSM-5 zeolite particles

Satoshi Inagaki, Shoma Shinoda, Shunsuke Hayashi, Yuji Nishita, Toru W ...

Session ID: 1A05
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_12

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A combination of mechanochemical bead-milling and the subsequent recrystallization treatment successfully yielded nano-sized ZSM-5 zeolite with high crystallinity. The acid treatment of nano-sized ZSM-5 zeolite removes framework Al selectively from the external surface, producing a unique ZSM-5 zeolite catalyst that has very few acid sites on its external surfaces. Such ZSM-5 nanoparticles showed higher propylene yield as well as high durability of coke formation during hexane cracking.

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Selective formation of propylene by dimethyl ether-to-olefin (DTO) reaction over dealuminated MCM-68 zeolite

Sungsik Park, Takuya Fukuoka, Satoshi Inagaki, Yoshihiro Kubota

Session ID: 1A06
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_13

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MCM-68 zeolites with various Si/Al molar ratios were prepared by dealumination with nitric acid. The amount of acid sites decreased with increasing HNO₃ concentrations while maintaining an intact framework of MSE topology. Catalytic performance of dealuminated MCM-68 zeolites for dimethyl ether (DME) conversion reactions into hydrocarbons showed a significant enhancement of propylene yield with high propylene/ethylene ratio in output products. On the basis of the results of NH₃-TPD and catalytic performance of the ion-exchanged and dealuminated MCM-68 zeolites, reducing acid amounts by dealumination is an important factor for the selective production of propylene by the DTO reaction.

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Incorporation of Al into iron-containing MFI zeolites and their catalytic activities on DTO reaction

Hiroki Kobayashi, Masafumi Nakaya, Kiyoshi Kanie, Atsushi Muramatsu

Session ID: 1A07
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_14

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Synthesis of furfurals from various saccharides over dealuminated Beta zeolite

Ryoichi Otomo, Toshiyuki Yokoi, Junko Nomura, Takashi Tatsumi

Session ID: 1A08
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_15

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[Award Lecture-The Japan Petroleum Institute Award for Encouragement of Research and Development]

Immobilization of molecular catalysts via a novel multipodal linker unit

Norihisa Fukaya

Session ID: 1A09
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_16

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[Regular Presentations]

Self-organization of gold nanoparticles induced by reversible photo-dimerization of organic protective agents

Keiko Miyabayashi, Shin-nosuke Hirai, Takahiro Hirasaki, Mikio Miyake

Session ID: 1A10
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_17

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Development of metal nanoparticle catalysts-supported on uncalcined mesoporous silica with the residual surfactant

Kohsuke Mori, Takuya Yamaguchi, Shohei Ikurumi, Hiromi Yamashita

Session ID: 1A11
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_18

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Highly efficient aerobic oxidation of various amines using Pd-based intermetallic compounds

Shinya Furukawa, Akifusa Suga, Takayuki Komatsu

Session ID: 1A12
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_19

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A series of Pd-based intermetallic compounds (ordered alloys) supported on SiO₂ were prepared and used for the aerobic oxidation of amines to imines. Pd₃Pb/SiO₂ showed a remarkably higher catalytic activity than monometallic Pd/SiO₂. Increase in basicity of catalyst support further enhanced the catalytic activity of Pd₃Pb. Nanoparticulate Pd₃Pb supported on Al₂O₃ can act as a highly efficient heterogeneous catalyst for the oxidation of various amines including primary, secondary, aromatic, aliphatic, and cyclic amines. A kinetic study revealed that the enhanced catalytic activity of Pd₃Pb was attributable to the promotion of imine desorption, which was the rate-determining step for the Pd catalyst. The enhancement in catalytic activity of Pd₃Pb with the basicity of support was attributed to the promotion of amine adsorption due to deprotonation by basic sites.

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Characterization and catalytic performance of TS-1 synthesized with various OSDAs

Toshiyuki Yokoi, Sayuri Katsuta, Junko Nomura, Takashi Tatsumi

Session ID: 1A13
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_20

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TS-1 has been used as a highly-efficient, heterogeneous catalyst for selective oxidation of organic compounds using hydrogen peroxide as oxidant. The catalytic activity of TS-1 strongly depends on the content and location of Ti atom in the framework, crystallinity, hydrophobicity, particle size and so on. These properties largely depend on a preparation method. In general, TS-1 is hydrothermally synthesized using tetraethyl orthosilicate (TEOS), titanium tetra-n-butoxide (TBOT), tetrapropylammonium hydroxide (TPAOH) as silica source, Ti source and structure-directing-agent, respectively. In this study, TS-1 zeolite was synthsized with pentaerythritol(PET) in the presence of n-butylamine.

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[Award Lecture-The Japan Petroleum Institute Award for Encouragement of Research and Development]

Development of highly active selective oxidation catalysts based on metal hydroxides and several new reactions

Kazuya Yamaguchi

Session ID: 1A14
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_21

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[Regular Presentations]

Effect of nickel plating condition on methane reforming property of a honeycomb-type Ni-based catalyst for hydrogen production

Kazumasa Yamamoto, Yudai Makiyama, Ryo Watanabe, Yoshiumi Kohno, Choji ...

Session ID: 1A15
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_22

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Study on catalytic properties of Rh-based intermetallic compounds in isomerization of cis-stilbene

Hui Luo, Shinya Furukawa, Kenichi Ozawa, Takayuki Komatsu

Session ID: 1A16
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_23

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We previously reported that Rh-based intermetallic compounds such as RhSb exhibited high selectivity in isomerization of cis-stilbene to trans-stilbene. In this study, we investigated the reason for the high selectivity in terms of geometric factors such as crystal structure of RhSb and its atomic arrangement of the surface.

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Effect of Ce addition on catalytic property of Ni/Al₂O₃ structured catalyst for steam reforming of naphthalene

Taiki Hata, Ryo Watanabe, Yoshiumi Kohno, Choji Fukuhara

Session ID: 1A17
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_24

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Catalytic property for dehydrogenation of propane in the presence of steam over Cr-based perovskite-type oxide

Ryo Watanabe, Masahiro Tsujioka, Yoshiumi Kohno, Choji Fukuhara

Session ID: 1A18
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_25

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Preparation of silica and silica-alumina with large mesopores using the gel skeletal reinforcement and estimation of catalytic cracking of n-dodecane

Hiroaki Oono, Tadanori Hashimoto, Hiroyuki Nasu, Atsushi Ishihara

Session ID: 1B01
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_26

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Silica and silica-alumina with large mesopores were pepared using the gel skeletal reinforcement and their reactivity as matrices were investigated in catalytic cracking of n-dodecane using mixed catalysts with zeolite. The mixed catalysts showed very high catalytic activity compared with those of zeolite singles.

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Catalytic cracking of heavy oils by zeolite containing microporous and mesoporous materials using a Curie point pyrolyzer

Takehiro Nakanishi, Tadanori Hashimoto, Hiroyuki Nasu, Atsushi Ishihar ...

Session ID: 1B02
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_27

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Catalytic cracking of heavy oils such as vacuum gas oil and atmospheric residue by zeolite containing microporous and mesoporous materials was investigated using a Curie point pyrolyzer.

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Aerobic oxidation of dibenzothiophenes in the presence of ruthenium catalysts

Yu Morishita, Satoru Murata, Satoshi Sunada

Session ID: 1B03
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_28

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Preparation and hydrodesulfurization activity of supported RuS₂ catalyst

Yasuharu Kanda, Toru Araki, Ayaka Sawada, Masatoshi Sugioka, Yoshio Ue ...

Session ID: 1B04
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_29

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Investigation of active site formation mechanism of hydrodesulfurization catalysts using the CVD method

Takeshi Nakabayashi, Kenichi Muramatsu, Takeshi Kubota, Kohji Omata, Y ...

Session ID: 1B05
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_30

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[Award Lecture-The Japan Petroleum Institute Award for Encouragement of Research and Development]

Studies on preparation and performance of noble metal phosphides as new hydrotreating catalysts

Yasuharu Kanda

Session ID: 1B06
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_31

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[Regular Presentations]

The present status and future image of the world offshore oil development

Masaru Ihara

Session ID: 1B07
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_32

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It is necessary to watch closely the fundamentals of the supply and demand, the access to oil resources, technical innovation, infrastructure, geopolitics, and an economic condition to understand ″the global status of the offshore oil field″. The current movement and the position of Japan on the global offshore oil development will be discussed.

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[Award Lecture-Noguchi Memorial Award for Encouragement of Reserch and Development]

Development of the FCA (fluid catalytic aromaforming) process

Shinichiro Yanagawa

Session ID: 1B08
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_33

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[Regular Presentations]

Acid catalysis of titanium-immobilized mesoporous silica for the Mukaiyama-aldol reastion in water

Kiyotaka Nakajima, Hiroshi Shintaku, Masaaki Kitano, Michikazu Hara

Session ID: 1B09
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_34

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Analysis of reaction mechanism of catalytic methane steam reforming at low temperature with an electric field

Yuusuke Sasaki, Ryo Manabe, Kazumasa Oshima, Shuhei Ogo, Yasushi Sekin ...

Session ID: 1B10
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_35

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Effects of an electric field in forward and reverse water gas shift reaction at low temperature

Koudai Yamagishi, Yukako Nogami, Kazumasa Oshima, Shuhei Ogo, Yasushi ...

Session ID: 1B11
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_36

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[Award Lecture-The Japan Petroleum Institute Award for Encouragement of Research and Development]

Development of novel carbon molecular sieve membranes and their application to membrane separation processes

Miki Yoshimune

Session ID: 1B12
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_37

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[Regular Presentations]

Membrane reactor process for hydrogen recovery from ammonia decomposition

Atsushi Oshima, Takafumi Sato, Naotsugu Itoh

Session ID: 1B13
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_38

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Development of carbon molecular sieve membranes for ultrapure hydrogen purification from organic chemical hydrides

Miki Yoshimune, Kenji Haraya

Session ID: 1B14
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_39

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Effects of Co addition to Ni catalyst on partial oxidation of methane

Yuji Kondo, Toshinari Eda, Daiki Mukai, Shuhei Ogo, Yasushi Sekine

Session ID: 1B15
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_40

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Combustion of diesel particulate over rare earth doped Co-Ce-based oxide catalyst

Hiroki Asajima, Hiroki Muroyama, Toshiaki Matsui, Koichi Eguchi

Session ID: 1B16
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_41

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Reaction mechanism of Pd/K/Co₃O₄ as a catalyst for water gas shift reaction

Yujin Kohno, Sakurako Tamura, Shuhei Ogo, Yasushi Sekine

Session ID: 1C01
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_42

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Catalytic methane dry reforming assisted by an electric field at low temperature

Kazumasa Oshima, Kei Sugiura, Tomohiro Yabe, Shuhei Ogo, Yasushi Sekin ...

Session ID: 1C02
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_43

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Directive methane conversion to high purity hydrogen with microwave heating

Akihiko Miyakoshi, Yutaka Akinaga, Daiki Yoshida

Session ID: 1C03
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_44

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Study on catalytic pyrolysis and zeolite regeneration

Kazuhisa Murata, Phunthinee Somwongsa, Isao Takahara, megumu Inaba, Ya ...

Session ID: 1C04
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_45

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Fast pyrolysis with three typical modified zeolite catalysts has been performed to produce bio-oil from jatropha waste. Jatropha waste was pyrolyzed in stainless-steel reactor at 600^oC under N₂ gas flow. Bio-oil with the highest aromatic hydrocarbon of 74% was prepared from pyrolysis using PtPd/ZSM(30) catalyst, where the weight ratio of jatropha/catalyst was 1. In addition to PtPd/ZSM(30), modified-Beta(22.5) and USY(20) were also screened and regenerated to study on the catalyst efficiency. The analysis of fresh and regenerated catalysts by XRD, NH₃-TPD, TG/DTG as well as product selectivity and textual properties shows that the behaviors for coke deposition and its removal would be associated with the zeolite structure and surface acid strength.

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Catalytic conversion of 2-octanol originating from plant oils to aromatic compounds

Ryota Takezawa, Masao Morimoto, Masakazu Iwamoto

Session ID: 1C05
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_46

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Catalytic conversions of sugars into light hydrocarbons over Pt/H-USY catalyst

Shuhei Ogo, Taku Nishio, Yasushi Sekine

Session ID: 1C06
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_47

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Selective hydrogenolysis of cyclic di-ols to mono-ols over Pd-W catalyst

Yoshinao Nakagawa, Yasushi Amada, Masazumi Tamura, Keiichi Tomishige

Session ID: 1C07
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_48

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Study on SOFC anodes based on pyrochlore oxides

Tomohito Sasouzaki, Daisuke Minori, Ryuji Kikuchi, Atsushi Takagaki, T ...

Session ID: 1C08
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_49

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The development of the solid acid catalyst for steam reforming of dimethyl ether for hydrogen production

Fumito Otsuka, Ryuji Kikuchi, Atsushi Takagaki, Takashi Sugawara, S.Te ...

Session ID: 1C09
Published: 2014
Released on J-STAGE: July 27, 2014

DOIhttps://doi.org/10.11523/sekiyu.2014.0_50

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