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58th R&D Symposium of the Japan Petroleum Institute

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Special Lecture

Future vehicles development at Honda

Yuji Kawaguchi

Session ID: S01
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.1.0

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Award Lecture

[Award Lecture-Noguchi Memorial Award]

Accomplishments of phase 1 of Japan's methane hydrate exploitation program

Shoichi Tanaka

Session ID: S02
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.2.0

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Accomplishments of phase 1 are summarized. Original in-place of methane included in hydrate formations in the Eastern Nankai Trough area wasestimated by probabilistic method. The second on-shore production test at Canada Arctic Circle on spring, 2008, successfully produced methane from hydrate formation for six days running by depressurization method.

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[Award Lecture-The Japan Petroleum Institute Award for Technological Progress]

The development and practical use of refrigeration lubricants for heat pump water heater system with CO₂

Masato Kaneko, Takeo Tokiai, Harutomo Ikeda

Session ID: S03
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.3.0

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Development and commercialization of FCC catalyst for the production of high octane gasoline

Katsuya Watanabe, Kenji Nagai, Hiroshi Mizutani, Yoshiyuki Toyooka

Session ID: S04
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.4.0

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[Award Lecture-The Japan Petroleum Institute Award]

Development of new propylene oxide process by cumene recycling

Tateo Seo, Masaru Ishino

Session ID: S05
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.5.0

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Shape-selective catalysis over zeolites -the alkylation of polynuclear hydrocarbons-

Yoshihiro Sugi

Session ID: S06
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.6.0

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Research on imine-based group 4 metal catalysts for olefin polymerization

Terunori Fujita

Session ID: S07
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.7.0

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Award Lecture

[Award Lecture-The Japan Petroleum Institute Award for Distinguished Papers]

Estimation of gas composition and cage occupancies in CH₄-C₂H₆ hydrates by CP-MAS ¹³C NMR technique

Masato Kida, Hirotoshi Sakagamai, Nobuo Takahashi, Akihiro Hachikubo, ...

Session ID: A01
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.8.0

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Rate-based modeling for internally heat-integrated distillation column (HIDiC) in binary system

Keigo Matsuda, Koichi Iwakabe, Kazuya Kubo, Akio Horiguchi, Weifang Yu ...

Session ID: A02
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.9.0

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A rate-based model of an internally heat-integrated distillation column (HIDiC) with structured packings was developed and the separation of benzene-toluene binary mixture was simulated. The developed model was applied to a bench-scale HIDiC to evaluate the separation and operation performance. The validity of the simulation results was confirmed with experimental data obtained from the HIDiC bench plant. The simulation results were also compared with those obtained from the conventional equilibrium model, which showed that the present model can predict the behavior of the bench plant more accurately than the conventional equilibrium model. The energy-saving ratio of the HIDiC system could also be investigated using this rate-based simulator.

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[Award Lecture-Noguchi Memorial Award for Encouragement of Research and Development]

Development of HDS catalyst for ultra low sulfur diesel by novel TiO₂ addition techniques

Narinobu Kagami

Session ID: A03
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.10.0

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[Award Lecture-The Japan Petroleum Institute Award for Encouragement of Research and Development]

Characterization of hydrodesulfurization catalysts by means of XAFS

Takeshi Kubota

Session ID: A04
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.11.0

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Design of transition metal oxide catalysts having uniform nano-structure and elucidation of their catalysis

Tetsuya Shishido

Session ID: A05
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.12.0

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Development of high-pressure chambers for DRIFT and XAFS spectroscopy, and their application to in-situ catalyst surface observation

Naoto Koizumi

Session ID: A06
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.13.0

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Partial oxidation of hydrocarbons with t -BuOOH catalyzed by V₂O₅ nano particules supported ionic liquid phase catalyst

Yuki Taniguchi, Yoshikazu Makioka

Session ID: A07
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.14.0

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Ethane selective oxidation in water over Mo₃VO_x mixed metal oxide catalysis

Takumi Fujisawa, Masahiro Sadakane, Wataru Ueda

Session ID: A08
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.15.0

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The design of catalytic membrane reactor for introducing hydroxy group into benzene

Masayuki Ishii, Kenichi Mimura, Takafumi Sato, Naotsugu Itoh

Session ID: A09
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.16.0

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Oxidative coupling of methane with modified La₂O₃ catalyst

Yasushi Sekine, Keisuke Tanaka, Masahiko Matsukata, Eiichi Kikuchi

Session ID: A10
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.17.0

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Oxidative Coupling of Methane (OCM) is a promising reaction to produce ethylene from natural gas in one step. Basic oxides are known to be effective catalysts for OCM. Especially, lanthanum oxide has high activity for OCM. Therefore, we investigated modifying lanthanum oxide with alkali-earth metal cation for high active/selective OCM catalyst. Among them, Ca and Sr improved the activity. It was inferred that the improvement of activity derived from enhancement of both basicity and oxygen defect on catalyst surface.

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Oxidation of thioethers catalyzed by V₂O₅ nano-particules

Yuki Taniguchi, Yoshikazu Makioka

Session ID: A11
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.18.0

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Low temperature catalytic reaction with electric field

Yasushi Sekine, Masayuki Haraguchi, Masahiko Tomioka, Masahiko Matsuka ...

Session ID: A12
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.19.0

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To achieve lower reaction temperature and higher conversion than existing catalytic processes for hydrogen production, catalytic reactions in an electric field for ethanol decomposition, steam reforming of ethanol, steam reforming of methane, water gas shift reaction were conducted. Conversion of reactant increased on catalytic reaction in an electric field by the interaction of electric field and catalyst. The activity was significantly improved with increasing current of the electric field.

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Conversion of gaseous hydrocarbons using atmospheric low frequency plasma-jet

Daisuke Fukuoka, Motoki Kobayashi, Kaoru Onoe

Session ID: A13
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.20.0

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Development of storage system of hydrogen derived from renewable energy by organic hydrides

Masahiro Kato, Masashi Sakuramoto

Session ID: A14
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.21.0

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Elucidation of saccharification mechanism of lignocellulose biomass using solid acid

Hirokazu Ariga, Satoshi Uehara, Eika Qian

Session ID: A15
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.22.0

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Photoinduced hydrogen production from polysaccharide and application to biomass fuel cell

Yutaka Amao, Yuka Sakai

Session ID: A16
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.23.0

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Dehydration and separation of trace amount of hazardous substances for bioethanol production

Hiroaki Habaki, Ryuichi Egashira

Session ID: A17
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.24.0

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Catalytic gasification of paper waste in high temperature liquid water

Aritomo Yamaguchi, Norihito Hiyoshi, Osamu Sato, Kyoko Bando, Masayuki ...

Session ID: A18
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.25.0

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Evertack : a special adhesive and high viscosity substance

Yoshihiro Goshi, Koichi Sato, Takahiro Kawaguchi, Minoru Hatayama

Session ID: B01
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.26.0

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Convert oilsand bitumen to ultra-clean transportation fuel

Kazuhiro Kashima, Tomoaki Hirano, Narinobu Kagami, Shigeyuki Mizuno, M ...

Session ID: B02
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.27.0

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Upgrading of hydrocracked product of heavy oil

Yoshikazu Sugimoto, Yukichi Horie

Session ID: B03
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.28.0

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Hydroctracking products ofheavy oil and straight-run VGO were hydrotreated, and the HDS and HDN reactivities were investigated in relation to the structure of the sulfur and nitrogen compounds in the feedstocks.

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Synchrotron radiation in-situ Ni, Mo K-edge EXAFS measurements of NiMo catalyst under high-presuure sulfiding condition

Yusuke Hamabe, Sungbong Jung, Yasuhiro Suzuki, Naoto Koizumi, Muneyosh ...

Session ID: B04
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.29.0

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4,6-DMDBT HDS activity of NiW catalyst prepared using novel SiO₂-Al₂O₃ support: Effect of modification with CyDTA

Shohei Yoshida, Naoto Koizumi, Muneyoshi Yamada

Session ID: B05
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.30.0

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Effect of deactivation conditions to simulate equilibrium catalyst on activity of FCC catalyst.

Norihito Chiyoda, Yuji Saka, Nobuki Sekine, Katsuya Watanabe

Session ID: B06
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.31.0

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Relationship between the shape of HDS catalyst and the fluid flow (Part2)

Yoshihiro Seriguchi, Nobumasa Nakajima, Takashi Fujikawa, Takeshige Ta ...

Session ID: B07
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.32.0

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Addition effect of boron and phosphorus on NiMo catalysts in hydrodenitrogenation of porphyrin

Eika W. Qian, Tetsuya Kurahashi, Satoshi Abe, Hiroyuki Ikeda

Session ID: B08
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.33.0

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Effect of pretreatment on activities of supported ruthenium hydrodesulfurization catalysts

Yasuharu Kanda, Taku Nakamura, Takao Kobayashi, Yoshio Uemichi, Masato ...

Session ID: B09
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.34.0

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Activities of supported Ru catalysts for hydrodesulfurization (HDS) were examined. The HDS activities of supported Ru catalysts were remarkably changed by various pretreatments. Especially, 5%Ru/Al₂O₃ treated by calcination at 200 ºC followed by sulfidation or temperature programmed sulfidation (TPS) using 3% H₂S-N₂ showed high activity for HDS of thiophene. Furthermore, HDS activity of 5%Ru/SiO₂ catalyst (calcined at 200 ºC) treated by TPS using 3% H₂S-N₂ was higher than those of 5%Ru/Al₂O₃ and CoMo/Al₂O₃ catalysts.

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Preparation of novel titania-supported cobalt-molybdenum catalysts using a sol-gel method and their hydrodesulfurization property

Atsushi Ishihara, Takahiro Saito, Shusaku Hayashi, Tadanori Hashimoto, ...

Session ID: B10
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.35.0

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Effect of citric acid addition on Co-Mo/(B)/Al₂O₃ catalysts prepared by a post-treatment method

Rinaldi Nino, Takeshi Kubota, Yasuaki Okamoto

Session ID: B11
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.36.0

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The effect of citric acid addition on a series of Co-Mo/(B)/Alumina catalysts prepared by a post-treatment method was studied for the HDS activity of thiophene. The catalysts were also prepared by a chemical vapor deposition (CVD) technique using Co(CO)₃NO as a precursor of Co. The prepared catalysts were characterized by means of NO and N₂ adsorption, LRS, EXAFS and UV-vis spectra. With a series of post-treated Co-Mo/(B)/Alumina catalysts, the HDS activity reached the maximum activity at the CA/Mo mole ratio of around 2. The addition of citric acid by the post-treatment significantly increased the HDS activity than by a simultaneous impregnation method, in particular at a 4 wt% Co-Mo/(B)/Alumina catalyst.

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Changes of hydrodesulfurization properties of ion-exchanged zeolite supported Co and Mo sulfide catalysts

Junichi Fukuma, Takeshi Kubota, Yasuaki Okamoto

Session ID: B12
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.37.0

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Dependence of activation energy for alkane cracking on Brønsted acid strength of zeolite

Naonobu Katada, Katsuki Suzuki, Takayuki Noda, Wataru Miyatani, German ...

Session ID: B13
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.38.0

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Synthesis of TS-1 in the presence of basic amino acids

Gou Kiyokawa, Toshiyuki Yokoi, Hiroyuki Imai, Junko Nomura, Takashi Ta ...

Session ID: B14
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.39.0

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Synthesis of 3D porous silica by assembling uniform-sized spherical silica particles.

Erina Kobayashi, Ryota Watanabe, Toshiyuki Yokoi, Takashi Tatsumi

Session ID: B15
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.40.0

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Synthesis of RTH-type zeolites under various conditions

Masato Yoshioka, Toshiyuki Yokoi, Hiroyuki Imai, Takashi Tatsumi

Session ID: B16
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.41.0

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Characterization of basic property of solid surface by a SO₂-TPD method

Ai Kuwahata, Takeshi Kubota, Yasuaki Okamoto

Session ID: B17
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.42.0

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Synthesis of nitrogen-doped zeolites and characterization as a base catalyst

Masaru Ogura, Taku Hasegawa

Session ID: B18
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.43.0

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Zeolites are used up to now in industrially important processes such as petro-refinary and petrochemistry. From now, other functions must be required to meet crisis of resources and materials, and to meet a demand on fine chemistry or some other new fields. Here, we focus on basicity of the material, contrary to the conventional acidic character of zeolites. A vast number of acid catalyses has been developed, while little is known on base catalyses. At our preliminary investigation step, zeolite-supported base oxides, -ion exchanged alkali, and a zeolite having nitrogen substituted with framework oxygen were adopted as candidates for base-catalyzed reaction such as Knoevenagel condensation. We found that nitrogen in the framework showed milder basicity than that induced by alkaline oxide or ion, and that high selectivity for condensed products was given.

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Influence of preparation factors on Ca/P ratio and surface basicity of hydroxyapatite catalyst

Takashi Tsuchida, Jun Kubo, Tetsuya Yoshioka, Shuji Sakuma, Tatsuya Ta ...

Session ID: B19
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.44.0

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Brønsted acid generation over alumina-supported niobia by calcination at 1173 K

Tetsuya Shishido, Tomoyuki Kitano, Kentaro Teramura, Tsunehiro Tanaka

Session ID: B20
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.45.0

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Development of Isooctene production technology by dimerization of butenes

Tatsuo Hamamatsu, Takashi Morikita, Nobuhiro Kimura

Session ID: B21
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.46.0

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Modification of sulfo group on delaminated MWW-type zeolite and its catalytic properties

Satoshi Inagaki, Yuko Kasama, Yoshihiro Kubota

Session ID: B22
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.47.0

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Preferential oligomerization of isobutene over sodium cation-modified H₄SiW₁₂O₄₀/SiO₂

Yuichi Kamiya, Jin Zhang, Ryuichiro Ohnishi

Session ID: B23
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.48.0

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Alkylation of isobutane with 1-butene over protonated zeolites

Yasushi Sekine, Yuichi Tajima, Yosuke Ichikawa, Masahiko Matsukata, Ei ...

Session ID: B24
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.49.0

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Novel solid acid catalysts are required instead of liquid acid catalysts based on green chemistry. In this work, various of zeolitc catalysts were examined for isobutane/1-butene alkylation to produce valuable fuel. We found that HBEA is more active than HZSM-5, HL and HY on this reaction.

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Deactivation and regeneration behaviors of copper spinel and zeolite composite catalysts in steam reforming of dimethyl ether

Naohiro Shimoda, Ryuji Kikuchi, Tetsuya Fukunaga, Koichi Eguchi

Session ID: C01
Published: 2009
Released on J-STAGE: July 19, 2009

DOIhttps://doi.org/10.11523/sekiyu.2009.0.50.0

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