日本応用磁気学会誌
Online ISSN : 1880-4004
Print ISSN : 0285-0192
ISSN-L : 0285-0192
21 巻, S_2_PMRC_97_2 号
選択された号の論文の120件中1~50を表示しています
Special invited session
Microstrure and micromagnetics
  • J.C. LODDER, S. de HAAN
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_17-30
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      The relation between deposition parameters, microstructural and magnetic properties are influencing the reversal mechanism of sputtered Co-Cr thin films having perpendicular anisotropy. Three Co-Cr films with perpendicular coercivities (Hc⊥) of 11, 90 and 170 kA/m are investigated. Besides the Hc⊥ several other parameters were studied by VSM, SEM, NMR, MFM, AFM, selective etching, such as the Hc⊥/Hk, Cr-segregation, domain structure, column sizes, etc.
    The anomalous Hall effect (AHE) has been used to record the hysteresis curves of sub-micron Hall crosses. This very sensitive technique in combination with e-beam lithography and ion-beam etching resulted in the recording of AHE hysteresis loops with dimensions of the Hall crosses as small as 0.3 × 0.3 μm2. The AHE-loops of three samples, with less than 60 columns, show different magnetic properties and the total number of steps measured in the hysteresis loop was 5 times the number of columns. The different reversal mechanism observed by the AHE are related to differences in microstructure, coercivity and domain size. The analysis of AHE hysteresis loops we conclude that magnetic units on the limit of superparamagnetism could be present in Co-Cr. The obtained results have been used as input for our model for micromagnetic simulations. Micromagnetic simulations shows that the initial layer and the exchange coupling of the initial layer with the columns has a large effect on the magnetisation reversal processes in the film.
  • Eiichi MIYASHITA, Yoshiro YONEDA, Junji NUMAZAWA
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_31-34
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Magnetization switching characteristics and recording/reproduction characteristics were calculated for a single layer perpendicular thin film medium with an initial layer. From calculation for various thicknesses of the medium, it was shown that the coercive force and reproduced signal output decrease substantially as the thickness of the initial layer is increased. Calculation of the aspect ratio of the fine particles included in the medium showed that the demagnetization effect is reduced when the aspect ratio of the fine particles is small.
  • Yoshihiro ISHII, Ken-ichi MINATO
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_35-38
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      A fanning mode in a columnar-structure film with perpendicular magnetization is studied on the assumption that the film is a two-dimensional array of prisms each of which consists of three identical single-domain grains. From the energy density, the nucleation fields HNfan for the fanning model and HNSW for the coherent-rotation mode are calculated. It is found that the difference between HNfan and HNSW is about 10% of them at the most. Furthermore the fanning mode occurs only for a very small range of the angle between the direction of the applied field and that of the easy axis of the magnetic uniaxial anisotropy normal to the film plane, and the exchange coupling at the granular interface further reduces this range. Therefore the fanning mode need not be taken into account in columnar-structured films used for perpendicular magnetic recording.
  • Hiroshi UCHIDA, Yoshiaki SONOBE, Yoshihiro IKEDA
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_39-42
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      To study the influence of thermal fluctuation in perpendicular recording media, we investigated a new incoherent magnetization model and combined it with the Langevin equation method. In our model, the energy barrier for magnetization reversal is reduced by using an incoherent reversal process. We simulated the M-H curve and the torque curve for perpendicular media with small Hc/Hk values, and calculated the time decay of Mr due to thermal fluctuation in the perpendicular media. The results roughly agreed with the experimental values of the time decay.
  • Eisuke SUZUKI, Yoichi HOSHI
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_43-46
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Sputter deposition process was investigated by computer simulation in order to clarify the effects of sputter-deposition parameters (sputtering gas pressure, substrate temperature, and high-energy particle bombardment of the film surface) on the microstructure of the film. Changes in sputtering gas pressure lead not only to changes in the distributions of the incidence angles and energy distribution of deposition particles, but also to changes in the film composition. The gas pressure dependence of the film composition in magnetron sputtering differs significantly from that in facing target sputtering. The surface migration of the deposited atoms due to thermally activated hopping leads to a considerable increase in film density. The bombardment of the film surface by high energy particles induces a significant migration of the deposited atoms and results in a dense structure.
  • Zhenghong Qian, John M. Sivertsen, Jack H. Judy
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_47-50
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      In this study, factors affecting magnetic properties of NiFe(100Å)/NiO(400Å) bilayers have been investigated. It’s found that magnetic properties of NiFe(100Å)/NiO(400Å) bilayers is not only dependent on the microstructure of bottom NiO layer but also dependent on the deposition condition of the top NiFe layer. Interfacial magnetic interaction of the bilayers is believed to play a critical role in controlling magnetic behavior of the bilayers. The measurement of the magnetic properties of NiFe(100Å)/NiO(400Å) bilayers showed them to be temperature dependent and also dependent on the in-plane angle of the applied field.
Media I : Oxide
  • Setsuo YAMAMOTO, Takayuki ANDOU, Nobuhiro KANAMARU, Tetsuya NAKAMURA, ...
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_51-56
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      A study on Co-γFe2O3/NiO perpendicular magnetic anisotropic media was reviewed focusing on their fabrication process, crystallographic and magnetic properties, and recording characteristics. The media were prepared using reactive sputtering in Ar+O2 mixture gas and annealing in air at lower process temperature than 350°C. The NiO underlayer deposited in room temperature had NaCl-like structure with <100> orientation. The Co-γFe2O3 layer prepared onto the NiO underlayer had also <100> orientation. The media have large perpendicular anisotropy energy of 1-3×106 erg/cm3 which was originated from preferential crystalline orientation of <100> axis of Co-γFe2O3and tensile stress at the Co-γFe2O3/NiO interface. The perpendicular coercivity of the media was widely changeable from 0.8 kOe to 6 kOe. The media was mechanically strong enough to use in sliding contact recording mode without protective overcoat layer. The media had excellent ultra-high-density recording performance, showing D50 over 150kFRPI and low media noise. It is concluded that the Co-γFe2O3/NiO medium is one of the promising candidates to achieve ultra-high-density recording.
  • Takanori DOI, Kousaku TAMARI, Yasuo KAKIHARA, Setsuo YAMAMOTO, Hiroki ...
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_57-60
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Co-γFe2O3 longitudinal magnetic recording media were prepared on NiO underlayer. Coercivity Hc was varied with Co content, atomic ratio of Co/Fe in Co-γFe2O3, and depositional O2 partial pressure. Hc of the media with Co/Fe=4 at% was 2000∼3500 Oe which were 1.3∼2.7 times higher than those of Co-γFe2O3 media without NiO underlayer. As concerns annealing temperature Ta, CoO-Fe3O4 films deposited on NiO were oxidized at lower Ta than that observed in the films on glass. Read/write characteristics of the media with no overcoat were evaluated in contact recording. Co-γFe2O3 media on NiO had higher and lower D50 and lower medium noise than those of the media without NiO underlayer.
  • H. Shimizu, H. Shinozaki, Y. Hoshi, K. Kato, F. Kaneko
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_61-64
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Deposition of c-axis perpendicularly oriented hexagonal barium ferrite thin films were formed by an alternate periodic deposition of S (Fe6O8) and R(BaFe6O11) layers. BaM film with excellent c-axis orientation and good crystallinity was obtained when S layers 4.7 Å thick and Rlayers 6.9 Å thick was deposited on a ZnO underlayer. To reduce the amount of the Zn ions diffusing from the ZnO underlayer to the BaM film, the thickness of the ZnO underlayer was reduced. An underlayer less than 10 nm thick, however, significantly degraded the c-axis orientation of the BaM films. We also tried to deposit BaM films on various kinds of underlayers such as α-Fe2O3 and amorphous barium ferrite (a-BaM). A BaM film with c-axis orientation was obtained only on a ZnO underlayer and an a-BaM/ZnO underlayer, although the c-axis of the BaM crystallites in the film deposited on a ZnO underlayer inclined about 2 degrees from the normal to the film surface.
  • Yingjian CHEN, James A. BAIN, Mark H. KRYDER
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_65-68
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Perpendicular barium hexaferrite thin films were fabricated using ex-situ and in-situ annealing. Our experimental results suggest that there are two different types of nucleation processes during the ex-situ annealing of the amorphous barium ferrite thin films. The nucleation within the film “bulk” tends to form crystallites with random c-axis orientations, whereas the nucleation at the interface(s) with the substrates or underlayers forms crystallites with the c-axis predominantly perpendicularly oriented. A Pt underlayer was shown to promote the interface nucleation which results in better perpendicular orientation. The barium ferrite films with Ba content higher than stoichiometry which were previously shown to have finer grain size, however, tend to grow grains of random orientation even on Pt underlayers due to the much enhanced “bulk” nucleation. Nearly perfect perpendicular orientation can be achieved in the high Ba content films if the films are made to be thin < 300 Å, and a two-step annealing is used. The films using in-situ annealing showed self-epitaxial growth of grains with perpendicular orientation, which can also be improved by using a Pt underlayer.
  • Fulin WEI, Mai LU, Changsheng WANG, Xiaoxi LIU, Zheng YANG
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_69-72
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      It was shown that the morphological and magnetic properties of Zn-Ti doped Ba-ferrite particles are suitable for magnetic recording. In order to clarify the temperature dependence of magnetic properties of these particles, BaFe10.8−2XZnX TiXO19 particles with the nominal composition X= 0.0-0.50 were prepared by synthesis from salt melts. The saturation magnetization Ms, magnetic anisotropy field HA and magnetocrystalline anisotropy constant K1 of above-mentioned particle assembly were estimated by using the law of approach to saturation of polycrystalline ferrite and the Curie temperature Tc was determined by the thermodynamic relation. With an increasing X, the Tc decreased, while the lattice parameter a, c and Ms have an unnoticeable maximum at X=0.20. The Hc(T) curves of samples with different X show that all particles have positive temperature coefficient in the vicinity of room temperature, which decreases with increasing X. The Ms(T), HA(T) and K1(T) were determined and discussed.
  • Tomoyosi SIOSAWA, Makoto ICHINOSE, Nobuhiro MATSUSHITA, Shigeki NAKAGA ...
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_73-76
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Ba ferrite/Pt bilayered films were deposited on thermally oxidized Si wafers using plasma-free sputtering method, and the dependence of crystallographical and magnetic characteristics on the substrate temperature Ts and the effectiveness of Pt underlayers were investigated. Ba ferrite films deposited at Ts above 500 °C revealed superior c-axis orientation even without post-annealing. Ba ferrite films deposited at Ts in the range from 200 to 450 °C revealed excellent c-axis orientation and exhibited extremely low coercivity after post-annealing at 800 °C. These results suggest that the Pt underlayers may be useful to reduce crystallization temperature of Ba ferrite films.
  • Nobuyuki HIRATSUKA, Eiichiro NIIZUMA, Koichi KAKIZAKI
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_77-80
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Barium ferrite films were prepared by r.f. diode sputtering on AlN underlayers, and then their crystal orientation and magnetic properties were investigated. The AlN underlayer with the thickness of about 5000Å which deposited at room temperature had well c-axis orientation. Furthermore the barium ferrite films were deposited on the AlN underlayer which had c-axis orientation. Because as-deposited barium ferrite films were not crystallized, the films were post-annealed at the temperatures between 600°C and 900°C for 5 hours in air. When the film was annealed at 650°C or more, the crystallinity of the hexagonal barium ferrite phase was improved and its [001] axis was oriented perpendicular to the film surface. It is considered that the superior orientation of [001] axis was the effect of AlN underlayer.
  • Yoshitaka KITAMOTO, Shusuke KANTAKE, Masanori ABE
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_81-84
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Ferrite-plated films were studied for application as perpendicular recording media. Though the ferrite plating has a merit of low temperature process below 100 °C, the microstructure must be improved for the media application. Power ultrasound irradiation into reaction solutions had effects on the reduction of grain size and the improvement of crystallinity maybe due to the increase of the nucleation sites on substrates and the acceleration of the ion migration in reaction. Doping Co2+ ions into Fe3O4 films increased perpendicular coercivity Hc⊥. CoxFe3-xO4 plated films of 70 nm in thickness around at x=0.5 had Hc⊥ of 2.8 kOe, Hc// of 0.6 kOe, and Ms of 450 emu/cc. Mossbauer analyses showed the films have perpendicular anisotropy.
  • Ferenc Vajda, Erik Samwel, Dennis Speliotis
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_85-94
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      In order to accurately measure the hysteresis parameters of recording media, it is necessary to control the operative field, h = H + αM, rather than the customary method of controlling the applied field, H. An automated iterative algorithm was implemented and tested that sets any prescribed value of h while ensuring that this target field is approached monotonically. The method was implemented on a DMS Vibrating Sample Magnetometer and experimentally tested on a commercial γ-Fe2O3 recording sample. The experimental results show that the new method gives substantially different minor loops than the corresponding customary measurement technique and could be used to automatically measure a recently proposed set of hysteresis parameters for recording media.
Head-media interface
Invited evening session
  • Dennis E. Speliotis
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_119-124
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Magnetic recording will be 100 years old next year and during that time it grew to become the main depository for information storage. In the arena of high performance rigid disks, areal densities have increased more than a million times since the appearance of the first disk drives some 40 years ago. The state of the technology will continue to grow from the present 2.6 Gbits/in2 to reach the celebrated goal of 10 Gits/in2 around the turn of the century. This goal will be achieved by evolutionary changes in the current longitudinal recording format. For the next stage of advancement to perhaps 30 Gbits/in2 more fundamental changes will be required, including perpendicular recording, oxide films, high saturation head materials, and the marriage with optics for high density tracking. Beyond 30 Gbits/in2 more revolutionary changes will be required, including patterned single domain nanoparticle arrays and near-field super-resolution optical probes. These innovations can eventually carry the technology to beyond 1 Tbit/in2!
Invited session : Progress of perpendicular magnetic recording and its issues
  • Yoshihisa NAKAMURA
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_125-134
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      First of all, it is confilrmed analytically that perpendicular magnetic recording has a much higher writing resolution which will reach a bit size corresponding to diameters of several magnetic particles when a sharper field gradient of a head and a narrower particle coercive force distribution of a medium are realized. After that, a writing head for perpendicular magnetic recording is discussed from a view point of the sharpness of the head field distribution around the trailing edge and the writing characteristics of a novel single-pole type flying head are presented. Furthermore, several technical issues for practical use of perpendicular magnetic recording such as media noise, thermal relaxation, head induced erasure and so on are discussed.
  • Bruce M. LAIRSON, Kuoksan HO, Shu-Yu SUN
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_135-139
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      Various properties of a vertical recording system comprising a merged MR head, a multilayer medium, and a soft magnetic underlayer were measured. SNR was found to be comparable to that of a high coercivity longitudinal disk, while nonlinearities were found to be much reduced. Measurements of nonlinear transition shift showed values less than 10% of the bit cell up to 390 kfci. Recording was performed using PR4 and EPR4 channels. Error rates below 1x10-7 could generally be obtained at low densities, which began to degrade above 300kfci. Using an EPR4 channel, an error rate of 4x10-4 was obtained at 350 kbpi at a data rate of 60 Mbits/sec.
  • Masaaki FUTAMOTO, Yoshiyuki HIRAYAMA, Yukio HONDA, Kenya ITO, Kazuetsu ...
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_141-149
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      This paper describes the recent research results on magnetic recording with single-layer perpendicular recording media. This includes the thermal stability of recorded information, the linear recording density resolution, the recorded track edge profile, the media noise, the nonlinear transition shifts, the signal decay due to demagnetizing field, etc. The combination of Co-alloy single-layer perpendicular media with high perpendicular magnetic anisotropies (Mr/Ms>0.95) and ring-head writing has a high potential to increase the attainable areal density beyond 10 Gb/in2 while avoiding or reducing the difficulties which are feared to face with the conventional longitudinal magnetic recording.
  • Yoshihiro IKEDA, Yoshiaki SONOBE, Hiroshi UCHIDA
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_151-156
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      A high signal-to-noise ratio (S/N) was achieved by increasing the Cr content of CoCr and CoCrPt perpendicular media. When the Cr content was increased from 22 at.% to 28 at.%, the S/N increased by 6 dB at 70 kFCI. Addition of 6 at.% Pt to the Co72Cr28 medium yielded a 2 dB higher S/N than that of a longitudinal medium. The medium noise was analyzed by using the parameters Ms, δM, and medium thickness. The medium noise of both CoCr and CoCrPt media increase with the Ms value increase. The existence of an anti-magnetized area in the dc-erased track may affect the increase in the noise of the perpendicular media. There are two types of medium thickness dependence of the S/N. The Cr-rich CoCr medium, whose S/N is maximized at a large medium thickness, is expected to be used for recording densities of over 10 Gbits/in2.
  • Hiroaki MURAOKA, Yoshihisa NAKAMURA
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_157-162
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      A quantitative calculation of the readback performance of shielded MR heads is performed for high density perpendicular magnetic recording, and compared with that from longitudinal recording. An analytical expression of the head field of the MR head with doule layer media is given to be used in a reciprocity calculation. Conditions to achieve a half-height pulse width, PW50' of 115 nm and 70 nm are presented. With these results and SNR estimations, issues of the read/write system to obtain areal densities of 20 Gbpsi and higher are discussed.
  • Katsumichi TAGAMI, Shinzo TSUBOI, Satoshi OHKI, Takahiro KORENARI, Tos ...
    1997 年 21 巻 S_2_PMRC_97_2 号 p. S2_163-168
    発行日: 1997年
    公開日: 2011/12/15
    ジャーナル オープンアクセス
      The read/write characteristics of a double-layered perpendicular magnetic recording medium were examined by using a combination of a single-pole-type write head and a magnetoresistive read head (SPT write / MR read), and a conventional merged ring type inductive / MR head (RT write / MR read). By differential equalization of the reproduced voltage, the STP/MR head combination had high density recording capability, compared with the RT/MR head. Bit error rate through PR(1) signal processing was evaluated for the SPT/MR head combination and the RT/MR head. It is clarified that bit error rate for the SPT/MR head combination and the RT/MR head. The bit error rate less than 10-6 at 3 Gb/inch2 was obtained for the SPT/MR head combination.
Media II : Thin film
Recording theories and characteristics
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