Journal of Surface Analysis
Online ISSN : 1347-8400
Print ISSN : 1341-1756
ISSN-L : 1341-1756
Volume 14, Issue 1
Displaying 1-5 of 5 articles from this issue
Paper
  • Adel Alkafri, Y. Ichikawa, R. Shimizu, K. Goto
    2007 Volume 14 Issue 1 Pages 2-8
    Published: 2007
    Released on J-STAGE: October 20, 2018
    JOURNAL FREE ACCESS

      We measured the transmission of the cylindrical mirror analyzer (CMA) by using a mini-electron gun consisting of a tungsten hairpin cathode set at the sample position. The electron beam current (iin) entering the CMA was measured using a retractable Faraday cup and an electrometer. The electrons get through the CMA and finally the detected current (iout) representing only a fraction of the input current was measured using another Faraday cup (normally used for detecting Auger electrons) and another electrometer. The ratio of the iout to iin gives the transmission of the CMA. Besides the experiment, we simulated the transmission characteristics, i.e., peak heights, position, and full width at half maximum, assuming thermionic emission and Gaussian peak shape. The simulation revealed characteristics that the experiments would not show explicitly. An optical transmission measurement was performed as well providing a good agreement with the results of the present electron beam measurements.

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  • I. Development of an Improved Backscattering Correction Equation for Wide Analytical Conditions
    S. Tanuma
    2007 Volume 14 Issue 1 Pages 9-19
    Published: 2007
    Released on J-STAGE: October 20, 2018
    JOURNAL FREE ACCESS

      This paper describes the backscattering correction for Auger quantitative surface analysis. The energy and electron incident angle dependence of backscattering coefficient for 10 elemental solids (Be, B, C, Al, Si, Cu, Zr, Ag, La, Au) were investigated using Monte Carlo (MC) simulations. In conclusions, the backscattering coefficient ηα at incident angle α could be described as

     

          ηα=(0.01η0−1.1+0.84)[η0/(0.01η0−1.1+0.84)]cosα

     

    where η0 is the backscattering coefficient at incident angle 0°. The Love-Scott equation [J. Phys. D 11, 106 (1978)] for η0 was superior to the others in wide incident energy range. Using these backscattering coefficient equations, we have proposed an improved equation for backscattering correction in Auger electron spectroscopy, which can be used for wide incident energy range (3-30 keV) and incident angles (0-60°). The parameters in the equation were determined from the curve fit to the backscattering factors at normal incident angle in the 3, 5, 7.5 and 10 keV electron incident energy calculated by Ichimura-Shizimu [Surf. Sci. 112, 386 (1981)] with MC method. The root mean square (RMS) differences for backscattering factors for 10 elemental solids calculated by Monte Carlo method using continuous slowing down approximation and those from proposed equation were less 3% in the 10-30 keV (over-voltage ratio U=1.5-100 and incident angle α=0-60°). In the 3-10 keV energy range, we have also compared the proposed equation to the calculated values at incident angle 30 and 45° by Ichimura-Shimizu with MC method. We found that they coincide well each other. Then, the proposed equation for backscattering correction could be applied to the quantitative Auger analysis in wide analytical conditions.

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