We investigated fluoride release and recharge capabilities of orthodontic resin containing surface pre-reacted glass-ionomer (S-PRG) filler, using 5 sets of 7-resin samples containing S-PRG filler at 0,5, 10, 20, or 30 wt%. Samples were immersed in distilled water from day 1 to 6. The water was changed every 24 hours and the amount of fluoride released was determined. From day 6 to 10, the samples were immersed in a fluoride solution (1,000 ppm) for 8 hours to recharge the fluoride and then in distilled water for 16 hours to determine the amount released. From day 11 to 15, the samples were again immersed in distilled water to estimate the fluoride release capabilities of the materials. Secondary electron images were obtained to assess the mixed state of the filler of a sample polymer containing 30 wt% S-PRG, while backscattered electron images were taken to observe the surface structure of the materials before and after the experiment.Our results revealed the following :1.Regardless of fluoride recharging, the amount of fluoride released was increased with an increasing percentage of S-PRG, with significant differences seen between 5 wt% and 20 wt%, 5 wt% and 30 wt%, and 10 wt% and 30 wt%.2.The amount of fluoride released appeared to decrease after repeated recharging. However, no significant reduction in the amount released was observed in samples containing 30 wt% S-PRG.3.Backscattered electron images obtained before and after the experiment showed uniformly dispersed S-PRG filler with occasional aggregates in polymerized resin. No filler fallout or breakdown was observed on the surface of the resin samples.
View full abstract