粉体および粉末冶金
Online ISSN : 1880-9014
Print ISSN : 0532-8799
ISSN-L : 0532-8799
12 巻, 3 号
選択された号の論文の4件中1~4を表示しています
  • 岡崎 千里
    1965 年 12 巻 3 号 p. 93-101
    発行日: 1965/06/25
    公開日: 2009/05/22
    ジャーナル フリー
  • 高間 栄三
    1965 年 12 巻 3 号 p. 102-107
    発行日: 1965/06/25
    公開日: 2009/12/04
    ジャーナル フリー
    To obtain ferrites which show rectangular hysteresis loops, MnO-ZnO-Fe2O3 ternary ferrites were sintered by the two step sintering process, wherein the first step sintering is performed under a reduced atmosphere and the second step sintering is done under an equilibrium atmosphere.
    Sintering process of the two step sintering was also studied.
    The results are as follows :
    1) Mn-Zn-Fe ferrites having rectangular hysteresis loops are obtained when the composition is such that λ 111 is small, and K 1 is adequately large.
    2) B r/B 5=0.94, B r=3, 890 Gauss, H c=0.37 Oe, T c=280°C and density=4.92 g/cc at the composition of 51 MnO-49Fe2O3.
    3) When ferrites are sintered under a reduced atmosphere, a considerable ferrite formation occurs at 1, 000°C, and a remarkable shrinkage proceeds over the temperature range between 1, 000°C and 1, 200°C.
  • W-NiP合金の焼結特性
    伊藤 普, 古川 満彦
    1965 年 12 巻 3 号 p. 108-115
    発行日: 1965/06/25
    公開日: 2009/05/22
    ジャーナル フリー
    The activated sintering of tungsten with Ni or other group VIII elements had been studied by J. H. Brophy and many other investigators. We tried the activated sintering of tungsten with Ni-P alloy by means of the electroless Ni plating on purpose to obtain effective results.
    In this experiment, we obtained tungsten compact of a density 18.5g/cm3 by sintering at 1, 000°C for 30 minutes.
    The sample used was 0.5μ W powder, with 0.19wt% Ni-P alloy.
    It was difficult to obtain the tungsten compact of a higher density than 18.5g/cm3, as the tungsten particle size was larger than 1.5μ. Studies on the shrinkage, density, hardness and microstructure, as well as the chemical analysis and X-ray analysis were made in order to the mechanism of the process.
  • 川北 公夫, 大塚 昭信, 津々見 雄文, 壇上 和美, 岡田 吉郎
    1965 年 12 巻 3 号 p. 116-122
    発行日: 1965/06/25
    公開日: 2009/05/22
    ジャーナル フリー
    The compression of spherical glass powders has been studied by static method in the pressure range 0-7.5 tons per cm2 (Fig.1). The results obtained are as follows.
    (1) During the compression process, the following distinct steps are observed (Photo. 1, 2) : (a) Packing without crushing (Initial stage of Fig. 2, 5, 6). (b) Sudden breakage of the particles and rapid diminution of apparent specific volume (Fig. 2, 5, 6). (c) Compaction of the crushed particles (Fig. 2, 3, 4, 5, 6, 11).
    (2) In the process of the compression of spherical glass powder, the relation between P, the applied pressure, and n, the porosity, is generally given by the following equation (Fig. 5, Table 1) :
    -(dn/dP)=k·nx
    where k and x are constants.
    (3) The effect of particle size on the breakage phenomena has been studied (Fig. 6, 7, 8). (a) The breakage pressure is higher for small particles than for large ones (Fig. 8, 9). (b) The degree of rapid volume change accompanying the sudden breakage increases with increasing of the particle diameter (Fig.10).
    (4) In the experiments of binary mixture which composed of two different particle sizes with different ratio of mixing, it has been observed that the rapid volume change accompanying the breakage of large particles occurs when the component of large particles is above about 70 percent by weight (Fig. 12, 13, 14).
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