To produce Al-Ni intermetallic compound, Al-42mass%Ni powder mixture was formed by back-forward extrusion at the temperature near to melting point of aluminum. The structure of alloy extruded at 910K consists of Al
3Ni, Al
3Ni
2 and eutectic structure. In the alloy extruded at 1010K, it consists of the intermetallic compound Al
3Ni and Al
3Ni
2. The volume fraction of each phase in the structure changes by the heat treatment, that is, the Al
3Ni phase increases with increase of heat-treating temperature and the eutectic structure disappears. High temperature deformation behaviors of these alloys were characterized by compressive test at various temperatures. The alloy of intermetallic compound containing the eutectic structure have large ductility, the eutectic structure transforms to Al
3Ni phase during the high temperature deformation and this transformation similarly occurs by the heat treatment at eutectic temperature. It was recognized that the compressive yield stresses in Al
3Ni and Al
3Ni
2 phases became higher with rising deformation temperature, it is referred to as "anomalous strengthening behavior of intermetallic compound".
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